Main Title |
Evaluation of methods for the determination of total organic halide in water and waste / |
Author |
Cole, T. F. ;
Berry, A. M. ;
Wilson, R. L.
|
CORP Author |
Battelle Columbus Labs., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH. |
Publisher |
U.S. Environmental Protection Agency, Office of Research and Development, Environmental Monitoring and Support Laboratory, |
Year Published |
1985 |
Report Number |
EPA/600-S4-85-011; PB85166304 |
Stock Number |
PB85-166304 |
OCLC Number |
320775487 |
Subjects |
Groundwater ;
Petroleum waste ;
Halides--Environmental aspects
|
Additional Subjects |
Halogen organic compounds ;
Ground water ;
Water analysis ;
Sampling ;
Neutron activation analysis ;
Colorimetric analysis ;
Performance evaluation ;
Water pollution detection ;
Liquid wastes ;
Oil wastes ;
Polychlorinated biphenyls
|
Internet Access |
|
Holdings |
Library |
Call Number |
Additional Info |
Location |
Last Modified |
Checkout Status |
EJBD |
EPA 600-S4-85-011 |
In Binder |
Headquarters Library/Washington,DC |
11/09/2018 |
ELBD ARCHIVE |
EPA 600-S4-85-011 |
In Binder Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
NTIS |
PB85-166304 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
Collation |
3 pages ; 28 cm |
Abstract |
Various methods for the determination of total organic halides (TOX) in groundwater and in waste oil samples have been evaluated. Of three inorganic halide species generation approaches and three inorganic halide determinative techniques evaluated for groundwater analyses, one combined approach using Schoeniger flask oxidation with colorimetric chloride determination was chosen for laboratory validation and method detection limit studies. Groundwater samples were also analyzed for TOX using neutron activation analysis. A method for analysis of oil samples which uses the sodium biphenyl reagent and a colorimetric chloride method was found to be unsatisfactory for the analysis of various oils spiked with PCBs due to interferences in the colorimetric determinative step which resulted in recoveries greater than 100%. |
Notes |
"EPA Project officer: Mr. Thomas Pressley." "Battelle Columbus Labs., OH"--Cover. "Prepared for Environmental Monitoring and Support Lab., Cincinnati, OH"--Cover. Includes bibliographical references. "EPA/600-S4-85-011." "March 1985." |
Place Published |
Cincinnati, Ohio |
Access Notes |
Also available on the Internet. |
Corporate Au Added Ent |
United States. Environmental Protection Agency. Office of Research and Development.; Environmental Monitoring Systems Laboratory (Cincinnati, Ohio); Battelle Memorial Institute. Columbus Laboratories. |
PUB Date Free Form |
1985 |
BIB Level |
m |
Cataloging Source |
OCLC/T |
OCLC Time Stamp |
20090511125647 |
Language |
eng |
Origin |
OCLC |
Type |
MERGE |
OCLC Rec Leader |
01663nam 2200385Ka 45020 |