Main Title |
Heated Purge and Trap Method Development and Testing. |
Author |
Lucas, S. V. ;
Burkholder, H. M. ;
|
CORP Author |
Battelle Columbus Div., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH. |
Year Published |
1988 |
Report Number |
EPA-68-03-3224; EPA/600/4-88/029; |
Stock Number |
PB88-242607 |
Additional Subjects |
Chemical analysis ;
Water pollution ;
Ketones ;
Mass spectroscopy ;
Gas chromatography ;
Purging ;
Traps ;
Desorption ;
Equipment ;
Methodology ;
Alcohols ;
Acrylonitride ;
Acroleins ;
Acetonitrile ;
Methacrylonitrile ;
Dioxanes ;
Organic nitrogen compounds ;
Oxygen heterocyclic compounds ;
Butanols ;
Methyl ethyl ketone ;
Aldehydes ;
Volatile organic compounds ;
Water pollution detection ;
Propionitrile ;
Isobutyl alcohol
|
Internet Access |
|
Holdings |
Library |
Call Number |
Additional Info |
Location |
Last Modified |
Checkout Status |
NTIS |
PB88-242607 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
Collation |
81p |
Abstract |
The goal of the research was to develop a heated purge and trap method that could be used in conjunction with SW-846 method 8240 for the analysis of volatile, water soluble Appendix VIII analytes. The developed method was validated according to a partial single laboratory method validation test to determine its performance characteristics using mass spectrometric detection. A group of 33 polar analytes comprising selected aldehydes, ketones, alcohols, ethers, nitriles, a thiol and 9 nitrogen bases were examined. The eight compounds found suitable for analysis for heated purge and trap were: acrolein, methacrylonitrile, acrylonitrile, acetonitrile, 2-butanone, 1,4-dioxane, isobutanol and propionitrile. |
Supplementary Notes |
Sponsored by Environmental Monitoring and Support Lab.-Cincinnati, OH. |
PUB Date Free Form |
Aug 88 |
Category Codes |
68D; 99A |
NTIS Prices |
PC A05/MF A01 |
Primary Description |
600/06 |
Document Type |
NT |
Cataloging Source |
NTIS/MT |
Control Number |
830228435 |
Origin |
NTIS |
Type |
CAT |