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Main Title Fabrication de Chloral, Deshydratation du Solvant (Manufacturing of Chloral, Dehydration by Means of a Solvent).
CORP Author Economic Commission for Europe (UN), Geneva (Switzerland). Working Party on Low and Non-Waste Technology and Re-Utilization and Recycling of Wastes.;Environmental Protection Agency, Washington, DC.
Publisher 1995
Year Published 1995
Stock Number PB95-233854
Additional Subjects Chlorine ; Dehydration ; Audits ; Solvents ; Foreign technology ; Chloral
Library Call Number Additional Info Location Last
NTIS  PB95-233854 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 14p
Abstract This audit presents the modification to the dehydration stage of the chloral manufacturing. Chloral synthesis is achieved by ethanol and chlorine reaction. The resulting product which is approximately 80% chloral is then dehydrated using a solvent. The conventional process uses concentrated sulfuric acid (oleum) for dehydration. The sulfuric acid in the conventional process is separated after the distillation step and then rejected. The solvent in the low-pollution process is recycled after distillation. The chloral is separated from chlorinated by-products which are used by the plant, and from water which is slightly acidic.
Supplementary Notes Text in French and English. Sponsored by Environmental Protection Agency, Washington, DC.
Category Codes 41E; 99B
NTIS Prices PC A03/MF A01
Primary Description 100/00
Document Type NT
Cataloging Source NTIS/MT
Control Number 521406380
Origin NTIS
Type CAT