Main Title |
Sensitizing the 4-Aminoantipyrine Reaction with Phenolic Materials for use in Water and Waste Analysis. |
Author |
Ettinge, M. B. ;
Ruchhof, C. C. ;
Lishk, R. J. ;
|
CORP Author |
Environmental Health Center, Cincinnati, Ohio. |
Year Published |
1950 |
Stock Number |
PB-216 759 |
Additional Subjects |
( Water analysis ;
Phenols) ;
( Colorimetric analysis ;
Phenols) ;
( Spectroscopic analysis ;
Phensols) ;
Dyes ;
Antipyrine/amino ;
Water pollution detection
|
Holdings |
Library |
Call Number |
Additional Info |
Location |
Last Modified |
Checkout Status |
NTIS |
PB-216 759 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
Collation |
38p |
Abstract |
The use of 4-aminoantipyrine was proposed by Emerson in a new color test for phenols. As outlined by Emerson, the essentials of the reaction consist of bringing together the phenolic material, the 4-aminoantipyrine and an alkaline oxidant in a solution of sufficiently high pH to prevent the formation of antipyrine red. Potassium ferricyanide was recommended as the oxidant. The work to be described has had two goals: Evaluation of the reaction variables which affect usage of Emerson's reagent for the determination of the simpler phenols; and Devising a procedure sufficiently sensitive to detect a one p.p.b. concentration of phenol. |