Record Display for the EPA National Library Catalog

RECORD NUMBER: 14 OF 133

Main Title Chromatographic Methods for Analysis of Ethylene Oxide in Emissions from Stationary Sources.
Author Margeson, J. H. ; Steger, J. L. ; Homolya, J. B. ;
CORP Author Radian Corp., Research Triangle Park, NC.;Environmental Protection Agency, Research Triangle Park, NC. Atmospheric Research and Exposure Assessment Lab.
Publisher c1990
Year Published 1990
Report Number EPA-68-02-4119; EPA/600/J-90/116;
Stock Number PB90-264144
Additional Subjects Chromatographic analysis ; Ethylene oxide ; Carcinogens ; Adsorbents ; Hospitals ; Sterilization ; Chemical plants ; Surface properties ; Reprints ; Stationary sources ; Indoor air pollution ; Health hazards
Holdings
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Status
NTIS  PB90-264144 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 8p
Abstract
Chromatographic methods of analysis with FID detection were investigated for quantitation of ethylene oxide in emissions from production plants and commercial sterilizers. A column with a stationary phase of 3% Carbowax 20M on 80/100 Chromsorb 101 was used to separate ethylene oxide from potential interferents in emissions from production plants. Two columns were found that allow accurate quantitation of ethylene oxide in emissions from commercial sterilizers. Both columns elute ethylene oxide before Freon 12, the diluent in the sterilization process. One column has a stationary phase of 1% SP-1000 on 60/80 Carbopack B and can be used to quantitate ethylene oxide over a wider range of concentrations than the other column, 5% Fluorcol (a fluorinated oil) on 60/80 Carbopack B. Graphitized carbon, the solid support in both of these columns, may be participating in the ethylene oxide-Freon 12 separation.