Office of Research and Development Publications

Analytical Protocol for VX Using Gas Chromatography/Mass Spectrometry (GC/MS)

Citation:

Campisano, R. Analytical Protocol for VX Using Gas Chromatography/Mass Spectrometry (GC/MS) . U.S. Environmental Protection Agency, Washington, DC, EPA/600/R-16/116, 2016.

Impact/Purpose:

This document is for the determination of the chemical warfare agent O-ethyl-S-(2-diisopropylaminoethyl)methyl-phosphonothiolate (VX). The procedures have been multi-laboratory tested for preparation and analysis of VX in soil, wipe, and water samples. This analytical protocol involves microscale extraction, followed by gas chromatography/mass spectrometry analysis to identify and measure VX. Soil and wipe extracts also might require a concentration step using nitrogen evaporation to achieve appropriate levels of quantitation.

Description:

Report

Record Details:

Record Type:DOCUMENT( PUBLISHED REPORT/ REPORT)
Product Published Date:09/20/2017
Record Last Revised:02/10/2020
OMB Category:Other
Record ID: 337633