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IN-SITU MONITORING OF PRODUCT STREAMS FROM A SPINNING TUBE-IN-TUBE REACTOR USING A METTLER-TOLEDO REACT-IR
Citation:
CISZEWSKI, J., W. KOWALCHYK, AND M. GONZALEZ. IN-SITU MONITORING OF PRODUCT STREAMS FROM A SPINNING TUBE-IN-TUBE REACTOR USING A METTLER-TOLEDO REACT-IR. Presented at 232nd American Chemical Society Fall 2006 National Meeting, San Francisco, CA, September 10 - 14, 2006.
Impact/Purpose:
To inform the public
Description:
A Mettler-Toledo ReactIR system has been used for in-line, real-time monitoring of the product stream from a spinning tube-in-tube reactor (STT®, Kreido Laboratories, Camarillo California). This combination of a process intensified continuous-flow reactor and an in-situ analytical system has allowed for the rapid optimization of process conditions in order to quickly maximize the conversion of starting materials to products in the STT®. This presentation will provide results on chemical reactions performed utilizing this reactor-instrument combination.