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OLS Field Name OLS Field Data
Main Title Methodology for Measurement of Polychlorinated Biphenyls in Ambient Air and Stationary Sources - A Review.
Author Margeson., John H. ;
CORP Author Environmental Monitoring and Support Lab., Research Triangle Park, N.C. Quality Assurance Branch.
Year Published 1977
Report Number EPA/600/4-77/021;
Stock Number PB-269 350
Additional Subjects Reviews ; Chlorine organic compounds ; Sampling ; Gas analysis ; Chemical analysis ; Monitoring ; Air pollution ; Polyurethane resins ; Foams ; Extraction ; Gas chromatography ; Electron capture ; Absorption ; Concentration(Composition) ; Physical properties ; Chemical properties ; Stationary sources ; Polychlorinated biphenyls ; Air pollution detection ; Aroclors ; Electron capture detectors ; Biphenyl/chloro
Library Call Number Additional Info Location Last
NTIS  PB-269 350 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/23/1988
Collation 39p
Abstract The state of development of methodology for measurement of polychlorinated biphenyls (PCBs) in ambient air and stationary sources was reviewed. The most promising method for ambient air measurements involves collection of PCBs on polyurethane foam, extraction with an organic solvent, removal of interferences by colum chromatography, and confirmation and analysis by electron-capture gas chromatography. Quantitation by perchlorination of PCBs to decachlorobipheny (DCB) is the most promising quantitation technique, but the procedure has not yet been perfected to the points are quantitatively converted to DCB. Perfection of this technique should allow for significant improvement in the quality of ambient PCB data being generated. Source and ambient methods differ mainly in sampling. Work on methodology for stationary sources is in the early stages of development and futher investigations are needed. The report contains 56 references.
Highlights Notes Discusses the methodology involving collection of PCBs on polyurethane foam, extraction with an organic solvent, removal of interferences by chromatography and analysis by electron-capture detectors.
NTIS Title Notes Final rept..
PUB Date Free Form Apr 77
Category Codes 7C; 14B; 68A#; 99A#
NTIS Prices PC A03/MF A01
Primary Description 600/08
Document Type NT
Cataloging Source NTIS/MT
Control Number 323720675
Origin NTIS
Type CAT