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RECORD NUMBER: 11 OF 266

OLS Field Name OLS Field Data
Main Title Analysis of Hazardous Waste and Environmental Extracts by Capillary Gas Chromatography/Fourier Transform Infrared Spectrometry and Capillary Gas Chromatography/Mass Spectrometry.
Author Gurka, D. F. ; Hiatt, M. ; Titus, R. ;
CORP Author Environmental Monitoring Systems Lab., Las Vegas, NV. ;Nevada Univ., Las Vegas.
Year Published 1984
Report Number EPA/600/J-84/286;
Stock Number PB85-198380
Additional Subjects Hazardous materials ; Environmental surveys ; Extraction ; Chemical analysis ; Comparison ; Gas chromatography ; Infrared spectroscopy ; Mass spectroscopy ; Sampling ; Reprints ; Fused silica capillary column gas chromatography ; Fourier transform spectroscopy
Holdings
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NTIS  PB85-198380 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/21/1988
Collation 11p
Abstract The relative sensitivities of fused-silica capillary column gas chromatography/Fourier transform infrared spectrometry (FSCC/GC/FT-IR) versus packed-column GC/FT-IR and FSCC/GC/FT-IR versus fused-silica capillary column gas chromatography/mass spectrometry (FSCC/GC/MS) were compared. As part of this study, complex environmental extracts were analyzed by both FSCC/GC/FT-IR and FSCC/GC/MS. The on-line library search results for both techniques were compared with the visually-checked spectral results for all FSCC/GC/FT-IR detectable analytes. Positive analyte identification depended strongly on sample preparation technique, search library content, chromatographic resolution and compound class. It was concluded that a target compound approach would not have utilized much of the available analyte information in these extracts.
Supplementary Notes Prepared in cooperation with Nevada Univ., Las Vegas.
Availability Notes Pub. in Analytical Chemistry 56, n7 p1102-1110 Jun 84.
NTIS Title Notes Journal article.
Title Annotations Reprint: Analysis of Hazardous Waste and Environmental Extracts by Capillary Gas Chromatography/Fourier Transform Infrared Spectrometry and Capillary Gas Chromatography/Mass Spectrometry.
PUB Date Free Form c1984
Category Codes 7D; 68; 99A
NTIS Prices Not available NTIS
Primary Description 600/07
Document Type NT
Cataloging Source NTIS/MT
Control Number 519925519
Origin NTIS
Type CAT