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RECORD NUMBER: 12 OF 15

OLS Field Name OLS Field Data
Main Title Pesticide Residue Analysis in Human Tissue by Combined Gas Chromatography-Mass Spectrometry.
Author Biros, Francis J. ; Walker., Annita C. ;
CORP Author Environmental Protection Agency, Perrine, Fla. Perrine Primate Lab.
Year Published 1970
Stock Number PB-275 500
Additional Subjects Pesticides ; Chemical analysis ; Gas chromatography ; Mass spectrometry ; Residues ; Humans ; Tissue extracts ; Chlorine organic compounds ; DDT ; Dieldrin ; Reprints ; Cyclohexane/hexachloro ; Lindane
Holdings
Library Call Number Additional Info Location Last
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Status
NTIS  PB-275 500 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/23/1988
Collation 5p
Abstract Pesticide residues in human adipose tissue and liver tissue samples were identified by mass spectrometry coupled with gas chromatography. An extensive extraction and cleanup procedure was adapted from existing analytical methods to separate pesticide residues from the tissue samples. Concentration of pesticides in tissue ranged from 0.073 to 28.7 ppm. Mass spectral data were computer-enhanced to identify heptachlor epoxide. Other pesticides confirmed included the beta-isomer of 1,2,3,4,5,6-hexachlorocyclohexane (HCH), several isomers and metabolites of p,p'-DDT, and dieldrin. Advantages, limitations, and suggested modifications for improving the combined gas chromatography-mass spectrometry technique for pesticide residue analysis are discussed.
Supplementary Notes Pub. in Jnl. of Agricultural and Food Chemistry, v18 n3 p425-429 1970.
Availability Notes Included in the report, Journal Articles on Pesticide Chemical Analysis. Group 2, PB-275 495.
Title Annotations Reprint: Pesticide Residue Analysis in Human Tissue by Combined Gas Chromatography-Mass Spectrometry,
PUB Date Free Form 23 Mar 70
Category Codes 7D; 6F; 99A; 57P
NTIS Prices (Order as PB-275 495, MF A01)
Primary Description 500/01
Document Type NT
Cataloging Source NTIS/MT
Control Number 323729541
Origin NTIS
Type CAT