| Main Title |
Volatile organic compounds in whole blood - determination by heated dynamic headspace purge and trap isotope dilution GC/MS / |
| Author |
Cramer, P. H. ;
Boggess, K. E. ;
Hosenfeld, J. M.
|
| Other Authors |
|
| CORP Author |
Midwest Research Inst., Kansas City, MO.;Environmental Protection Agency, Washington, DC. Office of Pesticides and Toxic Substances. |
| Publisher |
Office of Pesticide and Toxic Substances, |
| Year Published |
1987 |
| Report Number |
EPA/560/5-87/008; EPA-68-02-4252; Proj.; MRI-8822-A(01) |
| Stock Number |
PB88-102918 |
| OCLC Number |
18799741 |
| Additional Subjects |
Blood analysis ;
Toxicology ;
Gas chromatography ;
Mass spectroscopy ;
Isotopes ;
Labeled substances ;
Dilution ;
Purging ;
Traps ;
Volatile organic compounds ;
Toxic substances
|
| Internet Access |
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| EHAM |
EPA/560/5-87/008 |
|
Region 1 Library/Boston,MA |
05/25/2016 |
| EJED NPCD |
EPA 560/5-87-008 |
|
OCSPP Chemical Library/Washington,DC |
08/10/2001 |
| EJED |
EPA 560/5-87-008 |
|
OCSPP Chemical Library/Washington,DC |
08/10/2001 |
| ELBD ARCHIVE |
EPA 560-5-87-008 |
Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
DISPERSAL |
| EMBD |
PB88-102918 MF |
|
NRMRL/GWERD Library/Ada,OK |
06/26/1992 |
| ERAD |
EPA 560/5-87/008 |
|
Region 9 Library/San Francisco,CA |
11/27/1992 |
| ESAD |
EPA 560-5-87-008 |
|
Region 10 Library/Seattle,WA |
03/23/2010 |
| NTIS |
PB88-102918 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
32 pages |
| Abstract |
The method described was developed for the determination of a selected list of 30 organic compounds in whole human blood. The method is a heated dynamic head-space purge and trap gas chromatographic method using mass spectrometry in the limited mass scan mode. A whole blood sample is diluted with organic free water and the mixture fortified with isotopically labeled compounds. The mixture is subsequently heated to 50 deg C while stirred and the volatile components are purged from the mixture and collected on an adsorbent trap. The volatile compounds are thermally desorbed from the trap onto a wide-bore fused silica capillary column. Detection of the compounds is accomplished using mass spectrometry in the limited mass scan mode where only selected ions are scanned. Quantitation of the analytes is accomplished by using the specific ion responses from standards of the analytes and their corresponding labeled analogs or internal standards. |
| Notes |
"July 24, 1987." |
| Place Published |
Washington, D.C. |
| Supplementary Notes |
Sponsored by Environmental Protection Agency, Washington, DC. Office of Pesticides and Toxic Substances. |
| Access Notes |
Also available on the Internet. Viewed: 03/10/2005. |
| Corporate Au Added Ent |
United States. Environmental Protection Agency. Office of Pesticides and Toxic Substances. |
| PUB Date Free Form |
1987 |
| NTIS Prices |
PC A03/MF A01 |
| BIB Level |
m |
| Medium |
unmediated |
| Content |
text |
| Carrier |
volume |
| Cataloging Source |
OCLC/T |
| OCLC Time Stamp |
20160419142847 |
| Language |
eng |
| Origin |
OCLC |
| Type |
MERGE |
| OCLC Rec Leader |
00941cam 2200253Ka 45020 |
