| Main Title |
Method of Chromatographic Determination of Acrolein in the Presence of Aliphatic Aldehydes (Metod Khromatograficheskogo Opredeleniya Akroleina v Prisutstvii Alifaticheskikh Aldehidov). |
| Author |
Ipatova, S. A. ;
Deianova., E. V. ;
|
| CORP Author |
Environmental Protection Agency, Research Triangle Park, N.C. Translation Services Section. |
| Year Published |
1973 |
| Report Number |
EPA-HS-174; |
| Stock Number |
PB-259 698-T |
| Additional Subjects |
Gas chromatography ;
Acroleins ;
Gas analysis ;
Air pollution ;
Industrial wastes ;
Combustion products ;
Aldehydes ;
Nitrogen oxides ;
Translations ;
USSR ;
Air pollution detection
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| NTIS |
PB-259 698-T |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
8p |
| Abstract |
The authors have tested methods used in industrial-sanitary chemistry and have come to the conclusion that none of the colorimetric methods is suitable to analyze acrolein in the presence of aliphatic aldehydes and nitrogen oxides. They developed a fluorescent method of determining acrolein. The method involves separating and quantitatively determining acrolein with the aid of thin-layer chromatography in silicagel-gypsum. It has been established that formaldehyde, aromatic and saturated aliphatic aldehydes, amines, phenols and nitrogen peroxide do not disturb determination. Acetaldehyde and crotonic aldehyde are separated in chromatography, for the absorption of vapors of acrolein from the air a 0.25% solution of hydrochloric hydroxylamine and activated charcoal (AG-5) is recommended. |
| Supplementary Notes |
Trans. of Gigiena i Sanitariya (USSR) v38 (10) p65-67 Oct 73. |
| Title Annotations |
+++A Method of Chromatographic Determination of Acrolein in the Presence of Aliphatic Aldehydes (Metod Khromatograficheskogo Opredeleniya Akroleina v Prisutstvii Alifaticheskikh Aldehidov)--Translation. |
| PUB Date Free Form |
1973 |
| Category Codes |
13B; 7C; 99A; 68A |
| NTIS Prices |
PC A02/MF A01 |
| Document Type |
NT |
| Cataloging Source |
NTIS/MT |
| Control Number |
323703747 |
| Origin |
NTIS |
| Type |
CAT |
