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Main Title Capillary Column GC-MS Determination of 77 Purgeable Organic Compounds in Two Simulated Liquid Wastes.
Author Yancey, M. F. ; Kornfeld, R. A. ; Warner, J. S. ;
CORP Author Battelle Columbus Div., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH. Physical and Chemical Methods Branch.
Year Published 1988
Report Number EPA-68-03-3224; EPA/600/4-88/030;
Stock Number PB88-245881
Additional Subjects Water pollution detection ; Gas chromatography ; Mass spectroscopy ; Concentration(Composition) ; Environmental monitoring ; Determination ; Samples ; Simulation ; Effluents ; Water quality ; Standard deviation ; Volatile organic compounds
Internet Access
Description Access URL
Library Call Number Additional Info Location Last
NTIS  PB88-245881 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 80p
Abstract The suitability of purge-trap-desorb (PTD) procedures for determination of 84 volatile organic compounds with capillary column gas chromatograph (GC) and mass spectrometry (MS) was evaluated. After collecting GC-MS data not previously available for some analytes, 7 of the 84 compounds were eliminated from further consideration because of poor purging efficiency or analyte instability. For each of the remaining 77 compounds, the linear concentration range and detection limit were determined with data obtained by PTD GC-MS analysis of spiked reagent water. The criterion was met over a concentration range of at least two orders of magnitude for 56 of the 77 analytes, 1.5 orders of magnitude for 12 analytes, and 1 order of magnitude for 6 analytes. The criterion was not met for acetone, trichlorofluoromethane, and 2-chloro-1,3-butadiene. Method performance was assessed by analyzing eight replicate aliquots of two simulated liquid waste samples (a municipal sewage sludge leachate and water containing fulvic acid) containing analytes spiked at two concentrations.
Supplementary Notes Sponsored by Environmental Monitoring and Support Lab.-Cincinnati, OH. Physical and Chemical Methods Branch.
PUB Date Free Form Aug 88
Category Codes 68D; 99A
NTIS Prices PC A05/MF A01
Primary Description 600/06
Document Type NT
Cataloging Source NTIS/MT
Control Number 830230743
Origin NTIS
Type CAT