| Main Title |
Identification and analysis of polychlorinated biphenyls and other related chemicals in municipal sewage sludge samples / |
| Author |
Erickson, Mitchell D. ;
Pellizzari., Edo D.
|
| Other Authors |
|
| CORP Author |
Research Triangle Inst., Research Triangle Park, N.C.;Environmental Protection Agency, Washington, D.C. Office of Toxic Substances. |
| Publisher |
Research Triangle Institute, |
| Year Published |
1977 |
| Report Number |
68-01-1978; EPA 560/6-77-021; EPA-68-01-1978; EPA 560/1977 RTI/001 |
| Stock Number |
PB-273 192 |
| OCLC Number |
43256423 |
| Subjects |
Organochlorine compounds ;
Polychlorinated biphenyls ;
Sewage sludge--Analysis ;
Chemical compounds ;
Polychlorinated biphenyls (PCBs)
|
| Additional Subjects |
United States--Toxic Substances Control Act ;
Chemical analysis ;
Sludge ;
Chlorine organic compounds ;
Samples ;
Extraction ;
Gas chromatography ;
Mass spectroscopy ;
Laboratory equipment ;
Sampling ;
Polychlorinated biphenyls ;
Sewage sludge ;
Polychlorinated naphthalenes ;
Polychlorinated aniline ;
Benzene/chloro ;
Produces ;
Sulfate/dimethyl
|
| Internet Access |
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| EJBD |
TD767.4.R84 1977 |
|
Headquarters Library/Washington,DC |
08/21/2012 |
| EJED |
EPA 560/6-77-021 |
|
OCSPP Chemical Library/Washington,DC |
01/14/2000 |
| EJED |
EPA 560/1977 RTI/001 |
|
OCSPP Chemical Library/Washington,DC |
09/10/1999 |
| EKBD |
EPA-560/6-77-021 |
|
Research Triangle Park Library/RTP, NC |
05/30/2003 |
| ELBD ARCHIVE |
EPA 560-6-77-021 |
Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
| ESAD |
EPA 560-6-77-021 |
|
Region 10 Library/Seattle,WA |
08/28/2018 |
| NTIS |
PB-273 192 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
xiv, 143 pages : illustrations, charts ; 28 cm |
| Abstract |
Methods were developed for the extraction, clean-up and GC/MS analysis of polychlorinated biphenyls (PCBs) and related chemicals in municipal sludge samples. Each of the sludge samples received from nine major United States cities was processed to yield a neutral fraction and two acid fractions which were methylated with dimethylsulfate and diazomethane, respectively. Samples were cleaned up by silica gel column chromatography. A total of 35 chlorinated compounds were found in the full scan GC/MS analysis, including polychlorobiphenyls, polychloronaphthalenes, polychloroaniline, polychlorobenzene and DDE. Some chlorinated compounds remain unidentified. |
| Notes |
"U.S. Environmental Protection Agency, Office of Toxic Substances." "EPA 7560/6-77-021." "Contract No. 68-01-1978." "August 1977." "Project Officer: Dr. Vincent J. DeCarlo." |
| Place Published |
Research Triangle Park, NC |
| Corporate Au Added Ent |
United States. Environmental Protection Agency. Office of Toxic Substances.; Research Triangle Institute. |
| PUB Date Free Form |
1977 |
| NTIS Prices |
PC A08/MF A01 |
| BIB Level |
m |
| Medium |
unmediated |
| Content |
text |
| Carrier |
volume |
| Cataloging Source |
OCLC/T |
| Merged OCLC records |
42306357 |
| OCLC Time Stamp |
20180823050719 |
| Language |
eng |
| Origin |
OCLC |
| Type |
MERGE |
| OCLC Rec Leader |
02179cam 2200553Ia 45010 |
