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RECORD NUMBER: 32 OF 140

Main Title EPA method study 30, method 625 : base/neutrals, acids and pesticides /
CORP Author Radian Corp., Austin, TX.;Environmental Monitoring and Support Lab., Cincinnati, OH.
Publisher U.S. Environmental Protection Agency, Office of Research and Development, Environmental Monitoring and Support Laboratory,
Year Published 1984
Report Number EPA-68-03-3102; EPA-600/4-84-053;
Stock Number PB84-206572
OCLC Number 41214647
Subjects Water--Pollution--United States--Measurement ; Water quality management--United States ; Water--Pollution--Measurement
Additional Subjects Chemical analysis ; pH ; Pesticides ; Water analysis ; Gas chromatography ; Mass spectroscopy ; Sampling ; Water pollution ; Tables(Data) ; Saponification number ; Neutralizing ; Sediments ; EPA method 625 ; Water pollution detection ; Computer aided analysis
Internet Access
Description Access URL
https://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=9100R5AV.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EHAM  EPA-600/4-84-053 Region 1 Library/Boston,MA 05/25/2016
ESAD  EPA 600-4-84-053 Region 10 Library/Seattle,WA 05/23/2011
NTIS  PB84-206572 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 222 pages.
Abstract The work which is described in this report was performed for the purpose of validating, through an interlaboratory study, Method 625 for the analysis of the base/neutral, acid, and pesticide priority pollutants. This method is based on the extraction and concentration of the various analytes followed by their determination through gas chromatography using a low resolution mass spectrometer as the measuring device. Participating laboratories were selected based upon technical evaluation of proposals and upon the analyses results of prestudy samples. The laboratories were supplied with ampuls containing various concentrations of the pollutant compounds. These solutions were aliquoted into four different water types which were subsequently analyzed according to the appropriate method. In addition to the sample concentrates, each laboratory was supplied with an industrial effluent which was used to help determine false positive and false negative data. The data obtained from the interlaboratory study were analyzed employing a series of computer programs known as the Interlaboratory Method Validation Study (IMVS) system which was designed to implement ASTM procedure D2777.
Notes Cover title. "Jun 84." Photocopy.
Place Published Cincinnati, Ohio
Supplementary Notes Portions of this document are not fully legible.
Corporate Au Added Ent Radian Corporation.
Title Ser Add Ent Environmental monitoring series ; 84-053.; PB (Series) ; 84-206572.
NTIS Title Notes Project rept. Jan 82-Jun 83.
PUB Date Free Form 1984
Series Title Untraced EPA 600/4 ; 84-053\ PB ; 84-206572
Category Codes 7D; 68D; 68E; 99A
NTIS Prices PC A20/MF A01
Primary Description 600/06
BIB Level m
Medium unmediated
Content text
Carrier volume
Cataloging Source OCLC/T
Control Number 424418918
OCLC Time Stamp 20160419143840
Language eng
Origin OCLC
Type MERGE
OCLC Rec Leader 01403cam 2200361Ia 45020