| Main Title |
Evaluation of Gel Permeation Chromatography for Clean Up of Human Adipose Tissue Samples for GC/MS Analysis of Pesticides and Other Chemicals. |
| Author |
MacLeod, Kathryn E. ;
Hanisch, Robert C. ;
Lewis, Robert G. ;
|
| CORP Author |
Health Effects Research Lab., Research Triangle Park, NC. |
| Year Published |
1981 |
| Report Number |
EPA-600/J-82-005; |
| Stock Number |
PB82-246836 |
| Additional Subjects |
Pesticides ;
Chemical compounds ;
Chemical analysis ;
Tissues(Biology) ;
Gas chromatography ;
Mass spectroscopy ;
Halogen organic compounds ;
Humans ;
Toxicology ;
Reprints ;
Gel permeation chromatography ;
Polychlorinated biphenyls ;
Polybrominated biphenyls ;
Chlorinated napthalene
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| NTIS |
PB82-246836 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
5p |
| Abstract |
Gel permeation chromatography (GPC) has been evaluated for clean up of human adipose tissue sample extracts in preparation for confirmatory analysis by gas chromatography-mass spectrometry (GC/MS). Studies were conducted with standard solutions, fortified chicken fat, and actual human adipose tissue samples. Nearly quantitative removal of lipid material was achieved with minimal losses of 16 organochlorine pesticides and metabolites: two polychlorinated biphenyl (PCB) mixtures, two chlorinated napthalene (PCN) mixtures, and a polybrominated biphenyl (PBB) mixture. Mass spectra free from interferences were obtained over the mass range from 46 m/z to 560 m/z. |
| Supplementary Notes |
Pub. in Jnl. of Analytical Toxicology, v6 p38-40 Jan/Feb 82. |
| NTIS Title Notes |
Journal article. |
| Title Annotations |
Reprint: Evaluation of Gel Permeation Chromatography for Clean Up of Human Adipose Tissue Samples for GC/MS Analysis of Pesticides and Other Chemicals. |
| PUB Date Free Form |
28 Dec 81 |
| Category Codes |
7D; 6E; 6F; 6T; 68E; 99A; 57D; 57H; 57Y |
| NTIS Prices |
PC A02/MF A01 |
| Primary Description |
600/11 |
| Document Type |
NT |
| Cataloging Source |
NTIS/MT |
| Control Number |
323821682 |
| Origin |
NTIS |
| Type |
CAT |
