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OLS Field Name OLS Field Data
Main Title Evaluation of Gel Permeation Chromatography for Clean Up of Human Adipose Tissue Samples for GC/MS Analysis of Pesticides and Other Chemicals.
Author MacLeod, Kathryn E. ; Hanisch, Robert C. ; Lewis, Robert G. ;
CORP Author Health Effects Research Lab., Research Triangle Park, NC.
Year Published 1981
Report Number EPA-600/J-82-005;
Stock Number PB82-246836
Additional Subjects Pesticides ; Chemical compounds ; Chemical analysis ; Tissues(Biology) ; Gas chromatography ; Mass spectroscopy ; Halogen organic compounds ; Humans ; Toxicology ; Reprints ; Gel permeation chromatography ; Polychlorinated biphenyls ; Polybrominated biphenyls ; Chlorinated napthalene
Holdings
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Status
NTIS  PB82-246836 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. 06/23/1988
Collation 5p
Abstract Gel permeation chromatography (GPC) has been evaluated for clean up of human adipose tissue sample extracts in preparation for confirmatory analysis by gas chromatography-mass spectrometry (GC/MS). Studies were conducted with standard solutions, fortified chicken fat, and actual human adipose tissue samples. Nearly quantitative removal of lipid material was achieved with minimal losses of 16 organochlorine pesticides and metabolites: two polychlorinated biphenyl (PCB) mixtures, two chlorinated napthalene (PCN) mixtures, and a polybrominated biphenyl (PBB) mixture. Mass spectra free from interferences were obtained over the mass range from 46 m/z to 560 m/z.
Supplementary Notes Pub. in Jnl. of Analytical Toxicology, v6 p38-40 Jan/Feb 82.
NTIS Title Notes Journal article.
Title Annotations Reprint: Evaluation of Gel Permeation Chromatography for Clean Up of Human Adipose Tissue Samples for GC/MS Analysis of Pesticides and Other Chemicals.
PUB Date Free Form 28 Dec 81
Category Codes 7D; 6E; 6F; 6T; 68E; 99A; 57D; 57H; 57Y
NTIS Prices PC A02/MF A01
Primary Description 600/11
Document Type NT
Cataloging Source NTIS/MT
Control Number 323821682
Origin NTIS
Type CAT