| Main Title |
Synthesis of 2-Naphthalene-d7-Sulfonic Acid. |
| Author |
Sniegoski, L. T. ;
White, E. ;
Konash, P. L. ;
|
| CORP Author |
National Bureau of Standards, Washington, DC.;Environmental Protection Agency, Washington, DC. |
| Year Published |
1982 |
| Stock Number |
PB83-156976 |
| Additional Subjects |
Synthesis(Chemistry) ;
Standards ;
Chemical analysis ;
Gas chromatography ;
Mass spectroscopy ;
Reprints ;
Naphthalene sulfonic acid ;
High performance liquid chromatography
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| NTIS |
PB83-156976 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
8p |
| Abstract |
2-Naphthalene-d7-sulfonic acid, required as an internal standard for the analysis of organic compounds in water by gas chromatography/mass spectrometry, was synthesized in one step from commercially available naphthalene-d8 and sulfuric acid-d2. A high-performance liquid chromatographic method was developed to separate 1- and 2-naphthalene-d7-sulfonic acids. The electron impact mass spectrum and isotopic purity of the 2-naphthalene-d7-sulfonic acid were determined. |
| Supplementary Notes |
Sponsored in part by Environmental Protection Agency, Washington, DC. |
| Availability Notes |
Pub. in Journal of Labelled Compounds. Radiopharmaceutials XIX, n9 p1081-1087 1982. |
| NTIS Title Notes |
Final rept.. |
| Title Annotations |
Reprint: Synthesis of 2-Naphthalene-d7-Sulfonic Acid. |
| PUB Date Free Form |
1982 |
| Category Codes |
7D; 7C; 99D; 99A |
| NTIS Prices |
Not available NTIS |
| Document Type |
NT |
| Cataloging Source |
NTIS/MT |
| Control Number |
314721094 |
| Origin |
NTIS |
| Type |
CAT |
