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OLS Field Name OLS Field Data
Main Title Analysis of Chlorinated Herbicides by High-Performance Liquid Chromatography/Mass Spectrometry.
Author Jones, T. L. ; Betowski, L. D. ; Yinon., J. ;
CORP Author Environmental Monitoring Systems Lab., Las Vegas, NV. ;Weizmann Inst. of Science, Rehovoth (Israel). ;American Chemical Society, Washington, DC.
Publisher c1990
Year Published 1990
Report Number EPA/600/D-90/021;
Stock Number PB90-221698
Additional Subjects Herbicides ; Chemical analysis ; Chlorine organic compounds ; Liquid chromatography ; Mass spectroscopy ; Ionization ; Tables(Data) ; Reprints ;
Library Call Number Additional Info Location Last
NTIS  PB90-221698 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. 08/27/1990
Collation 14p
Abstract A method that uses high performance liquid chromatography/mass spectrometry (HPLC/MS) for the analysis of chlorinated phenoxyacid herbicides is described. During method development different techniques were used to increase both the sensitivity and the specificity of thermospray HPLC/MS for chlorinated acid herbicides. These included the operation of the instrument in the negative chemical ionization (NCI) mode initiated by discharge and the use of a wire-repeller in the ion source for efficient extraction of positive ions. Single quadrupole repeller-induced and multiple quadrupole collision activated dissociation (CAD) experiments were also performed to increase the structural information of the mass spectra. The method complements the U.S. Environmental Protection Agency's gas chromatographic (GC) SW-846 Method 8151 for the determination of chlorinated acid herbicides.
Supplementary Notes Pub. in ACS Symposium Series No. 420, Liquid Chromatography/Mass Spectrometry: Applications in Agricultural, Pharmaceutical, and Environmental Chemistry, 1990. Presented at the National Meeting of the American Chemical Society (197th), Dallas, TX., April 9-14, 1989. Prepared in cooperation with Weizmann Inst. of Science, Rehovoth (Israel), and American Chemical Society, Washington, DC.
NTIS Title Notes Book chapter.
Title Annotations Reprint: Analysis of Chlorinated Herbicides by High-Performance Liquid Chromatography/Mass Spectrometry.
Category Codes 99A
NTIS Prices PC A03/MF A01
Primary Description 600/07
Document Type NT
Cataloging Source NTIS/MT
Control Number 019413984
Origin NTIS
Type CAT