Main Title |
Fused silica capillary column GC/MS quality control protocol for the determination of semivolatile priority pollutants. |
CORP Author |
Acurex Corporation. |
Publisher |
Environmental Monitoring Systems Lab., |
Year Published |
1984 |
Report Number |
EPA 600-4-84-068; EPA-68-03-3100 |
Stock Number |
PB 84-224-674 |
OCLC Number |
15430675 |
Additional Subjects |
Chemical analysis ;
Laboratory equipment ;
Quality control ;
Environmental surveys ;
Capillary tubes ;
Gas chromatography ;
Mass spectroscopy ;
Sampling ;
Calibrating ;
Performance evaluation ;
Standards ;
Pesticides ;
Organic compounds
|
Internet Access |
|
Holdings |
Library |
Call Number |
Additional Info |
Location |
Last Modified |
Checkout Status |
EJBD |
EPA 600-4-84-068 |
|
Headquarters Library/Washington,DC |
04/18/2018 |
NTIS |
PB84-224674 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
Collation |
57 pages tbls., graphs |
Abstract |
This quality control protocol is intended to serve as a guide to those laboratories employing fused silica capillary column (FSCC) gas chromatographic/mass spectrometric (GC/MS) techniques for the analysis of the extractable semivolatile priority pollutants. The document presents apparatus requirements and gives guidance for standards preparation, extract mixing, system setup and calibration. Qualitative and quantitative data including internal standard assignment, quantitation mass, relative retention times (RRT) values, interlaboratory and intralaboratory response factors (RF) values are also presented. This document provides a schedule for GC/MS system calibration requirements including: ion abundance calibration, column performance testing, sensitivity verification, system linearity, and injection technique reproducibility. This protocol does not provide guidance regarding sample extraction and workup; therefore, any quality control (QC) parameters related to this aspect of priority pollutant analysis are not addressed in this protocol. |
Notes |
"EPA 600-4-84-068." "July 1984." Cover title. |
Place Published |
Las Vegas, |
PUB Date Free Form |
1984 |
NTIS Prices |
PC A04/MF A01 |
BIB Level |
m |
Medium |
unmediated |
Content |
text |
Carrier |
volume |
Cataloging Source |
OCLC/T |
OCLC Time Stamp |
20180411074250 |
Language |
eng |
Origin |
OCLC |
Type |
MERGE |
OCLC Rec Leader |
00951cam 2200301K 45010 |