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RECORD NUMBER: 94 OF 107

Main Title Synthesis of DDT Labeled with Carbon-14 in the Tertiary Position.
Author Pearce, George W. ; Jensen., Jens A. ;
CORP Author Communicable Disease Center, Savannah, Ga.
Year Published 1952
Stock Number PB-274 735
Additional Subjects Synthesis(Chemistry) ; Pesticides ; DDT ; Chlorine organic compounds ; Isotopic labeling ; Carbon 14 ; Insecticides ; Reprints
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NTIS  PB-274 735 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 1p
Abstract A method has been developed for the synthesis of radioactive Dichlorodiphenyltrichloroethane (DDT) in good yield in which the tertiary carbon is labeled. Fields et al. have developed a satisfactory procedure for incorporating C(14) in the benzene ring. This procedure presumably was employed in a previously reported labeling of DDT with C(14). However, the complete synthesis of DDT by this procedure would involve at least seven major steps, with the consequent tendency towards low over-all yields. In the authors' procedure, only four major steps are necessary.
Supplementary Notes Pub. in Science, v118 n3054 p45-46, 10 Jul 53.
Availability Notes Included in the report, Journal Articles on Pesticide Chemistry, PB-274 732.
Title Annotations Reprint: Synthesis of DDT Labeled with Carbon-14 in the Tertiary Position,
PUB Date Free Form 15 Dec 52
Category Codes 7C; 6F; 18B; 99D; 57P; 77B
NTIS Prices (Order as PB-274 732, MF A01)
Primary Description 500/01
Document Type NT
Cataloging Source NTIS/MT
Control Number 323728436
Origin NTIS
Type CAT