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RECORD NUMBER: 280 OF 1267

Main Title Determination of 2,3,7,8-TCDD (Tetrachlorodibenzo-p-Dioxin) in Industrial and Municipal Wastewaters, Method 613. Part 1. Development and Detection Limits.
Author Longbottom, J. E. ; Foerst, D. L. ; Wesselman, R. J. ; Wong, A. S. ; McMillin, C. R. ;
CORP Author Environmental Monitoring and Support Lab.-Cincinnati, OH.
Year Published 1983
Report Number EPA-600/D-83-020;
Stock Number PB83-171280
Additional Subjects Water analysis ; Industrial wastes ; Sewage ; Pesticides ; Herbicides ; Chemical analysis ; Chlorine organic compounds ; Solvent extraction ; Gas chromatography ; Mass spectroscopy ; Reprints ; Dibenzodioxin/tetrachloro ; Water pollution detection
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Status
NTIS  PB83-171280 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 26p
Abstract A convenient method for water and wastewater samples is presented that will determine 2,3,7,8-TCDD concentrations to a Method Detection Limit (MDL) of 2 ng/L. The method uses solvent extraction of the aqueous sample followed by capillary column gas chromatography/mass spectrometry using Selected Ion Monitoring. The capillary column (Silar 10C or equivalent) is isomer specific for 2,3,7,8-TCDD.
Supplementary Notes Prepared in cooperation with California Analytical Lab., Inc., Sacramento, CA., and Monsanto Research Corp., Dayton, OH. Dayton Lab.
Title Annotations Reprint: Determination of 2,3,7,8-TCDD (Tetrachlorodibenzo-p-Dioxin) in Industrial and Municipal Wastewaters, Method 613. Part 1. Development and Detection Limits,
PUB Date Free Form 1983
Category Codes 7D; 68E; 99A; 68D
NTIS Prices PC A03/MF A01
Primary Description 600/06
Document Type NT
Cataloging Source NTIS/MT
Control Number 311919671
Origin NTIS
Type CAT