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RECORD NUMBER: 977 OF 995

Main Title Using Method 301 to Validate Sampling and Analytical Methods for Selected CAAA Compounds.
Author Jackson, M. D. ; Merrill, R. G. ; Bursey, J. T. ;
CORP Author Radian Corp., Research Triangle Park, NC.;Environmental Protection Agency, Research Triangle Park, NC. Atmospheric Research and Exposure Assessment Lab.
Publisher 1993
Year Published 1993
Report Number EPA-68-D1-0010; EPA/600/A-93/106;
Stock Number PB93-191419
Additional Subjects Air pollution monitoring ; Stationary pollutant sources ; Field tests ; Organic compounds ; Validation ; Precision ; Emission factors ; Clean Air Act Amendments of 1990 ; EPA Method 301
Internet Access
Description Access URL
https://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=P100VIAW.PDF
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Library Call Number Additional Info Location Last
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Status
NTIS  PB93-191419 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 12p
Abstract Stationary source sampling and analysis methods can be validated for a set of analytes and stack conditions using EPA Method 301 before these methods are used to comply with the requirements of the Clean Air Act Amendments of 1990. Most method validations require spiking of analytes under field conditions by gaseous dynamic spiking into two of four sampling trains on a quadruple probe (used with VOST), liquid spiking into two of four sampling trains using a quadruple probe (SemiVOST), and spiking of various analytes onto filters. A quadruple sampling probe with four trains is usually used to minimize the number of sampling runs needed to provide sufficient replicates for statistical calculations. Laboratory testing establishes experimental parameters such as stability, analytical method performance, sample preparation procedures, spiking conditions, and precision and accuracy of analysis. Successful laboratory testing supports a full field validation to evaluate the applicability of a given method to a particular analyte.
Supplementary Notes See also PB91-216184. Sponsored by Environmental Protection Agency, Research Triangle Park, NC. Atmospheric Research and Exposure Assessment Lab.
Category Codes 68A
NTIS Prices PC A03/MF A01
Primary Description 600/09
Document Type NT
Cataloging Source NTIS/MT
Control Number 318931135
Origin NTIS
Type CAT