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Main Title Thermospray LC/MS/MS Analysis of Wastewater for Disperse Azo Dyes.
Author Betowski, L. D. ; Pyle, S. M. ; Ballard, J. M. ; Shaul, G. M. ;
CORP Author Environmental Monitoring Systems Lab., Las Vegas, NV. ;Lockheed Engineering and Management Services Co., Inc., Las Vegas, NV.
Year Published 1987
Report Number EPA/600/J-87/184;
Stock Number PB88-161856
Additional Subjects Waste water ; Azo dyes ; Effluents ; Sludges ; Mass spectroscopy ; Dispersion ; Water pollution ; Reprints ;
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NTIS  PB88-161856 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 13p
Abstract Primary effluent from a municipal wastewater treatment plant was used as the feed in bench scale activated sludge systems. These systems were spiked with disperse azo dyes and were sampled at various points in the process. Samples were analyzed by high performance liquid chromatography with UV-visible detection and by thermospray ionization MS and tandem mass spectrometry (MS/MS) using direct injection or via column chromatography. The tandem mass spectrometry techniques were used both for method development purposes and for the specificity and extra information these techniques can provide. The investigation of the fate of disperse azo dyes in the activated sludge process was a major feature of the study. Major degradation products have been identified by tandem mass spectrometry analyses of these wastewaters. Precision and accuracy data generated by the thermospray tandem mass spectrometry technique are compared to those derived from the high performance liquid chromatography/UV-visible method. (Copyright (c) Biomedical + Environmental Mass Spectrometry, 14: 343-354, 1987.)
Supplementary Notes Pub. in Biomedical and Environmental Mass Spectrometry, v14 p343-354 1987. Prepared in cooperation with Lockheed Engineering and Management Services Co., Inc., Las Vegas, NV.
NTIS Title Notes Journal article.
Title Annotations Reprint: Thermospray LC/MS/MS Analysis of Wastewater for Disperse Azo Dyes.
PUB Date Free Form c1987
Category Codes 68D; 99A
NTIS Prices PC A03/MF A01
Primary Description 600/07
Document Type NT
Cataloging Source NTIS/MT
Control Number 809821975
Origin NTIS
Type CAT