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RECORD NUMBER: 107 OF 168

Main Title Mass Spectrometric Quantification of Polychlorinated Biphenyl Congeners Using Multiple Carbon-13 Internal Standards.
Author Shore, F. L. ; Martin, J. D. ; Williams, L. R. ;
CORP Author Environmental Monitoring Systems Lab., Las Vegas, NV. ;Lockheed Engineering and Management Services Co., Inc., Las Vegas, NV.
Year Published 1986
Report Number EPA/600/J-86/034;
Stock Number PB86-190097
Additional Subjects Synthesis(Chemistry) ; Spectrochemical analysis ; Chlorine organic compounds ; Standards ; Mass spectrometry ; Polychlorinated biphenyls
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NTIS  PB86-190097 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 8p
Abstract Multiple carbon-13 internal standards improve the precision and accuracy of the mass spectrometric analysis of polychlorinatedbiphenyl (PCB) congeners compared to analyses using a single carbon-13 internal standard. The mean percentage error in PCB congener analysis on the micrograms g-1 level using multiple ion detection and three carbon-13 internal standards was 6.29 percent. This precision in single laboratory work suggests that the method will be useful for interlaboratory studies monitoring PCB residues and contaminants of public health significance.
Supplementary Notes Pub. in Biomedical Mass Spectrometry, v13 n1 p15-19 Jan 86. Prepared in cooperation with Lockheed Engineering and Management Services Co., Inc., Las Vegas, NV.
NTIS Title Notes Journal article.
PUB Date Free Form c1986
Category Codes 7C; 7D; 68; 99D; 99F
NTIS Prices PC A02/MF A01
Primary Description 600/07
Document Type NT
Cataloging Source NTIS/MT
Control Number 617121906
Origin NTIS
Type CAT