| Main Title |
A one step method for the determination of carbamate pesticides by derivatization with [alpha]-bromo-2,3,4,5,6-pentafluorotoluene / |
| Author |
Jackson, Merrill D. ;
Soileau, Stephen D. ;
Sovocool, G. Wayne ;
Sachleben, Richard A.
|
| Other Authors |
|
| CORP Author |
Health Effects Research Lab., Research Triangle Park, NC. Analytical Chemistry Branch. |
| Publisher |
Health Effects Research Laboratory, Office of Research and Development, U.S. Environmental Protection Agency, |
| Year Published |
1979 |
| Report Number |
EPA-600/4-79-077; EPA-600/4-79-036 [printing error - use 077] |
| Stock Number |
PB80-142847 |
| OCLC Number |
34707162 |
| Additional Subjects |
Pesticides ;
Carbamates ;
Chemical analysis ;
Trace elements ;
Hydrolysis ;
Bromine organic compounds ;
Gas chromatography ;
Toluene/bromo-pentafluoro ;
Procedures
|
| Internet Access |
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| EJBD |
EPA 600-4-79-077 |
|
Headquarters Library/Washington,DC |
03/22/2016 |
| EKBD |
EPA-600/4-79-077 |
|
Research Triangle Park Library/RTP, NC |
05/10/1996 |
| EKCD |
EPA-600/4-79-077 |
|
CEMM/GEMMD Library/Gulf Breeze,FL |
07/25/2018 |
| ELBD ARCHIVE |
EPA 600-4-79-077 |
Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
| EMBD |
EPA/600/4-79/077 |
|
NRMRL/GWERD Library/Ada,OK |
05/24/1996 |
| ESAD |
EPA 600-4-79-077 |
|
Region 10 Library/Seattle,WA |
03/23/2010 |
| NTIS |
PB80-142847 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
vii, 95 pages : illustrations ; 28 cm. |
| Abstract |
A procedure was developed for the determination of trace quantities of a broad range of carbamate pesticides. The carbamates were hydrolyzed and derivatized in a single step, using alkali and alpha-bromo-2,3,4,5,6-pentafluorotoluene (PFBB), and were subsequently analyzed using electron capture gas chromatography. This one step derivatization method created a novel derivative in which one fluorine on the PFB ring was displaced by an ethoxide ion via aromatic nucleophilic substitution. |
| Notes |
"By Merrill D. Jackson, Stephen D. Soileau, G. Wayne Sovocool and Richard A. Sachleben, Environmental Toxicology Division, Health Effects Research Laboratory." Document no. changed after publication to EPA-600/4-79-077. No. EPA-600/4-79-036 belongs to title "Hydraulics of the Atchafalaya basin ..." (OCLC #5397078). "September 1979." Includes bibliographical references (pages 20-22). |
| Place Published |
Research Triangle Park, N.C. |
| Corporate Au Added Ent |
Health Effects Research Laboratory (Research Triangle Park, N.C.). Environmental Toxicology Division.; United States. Environmental Protection Agency. Office of Research and Development. |
| Title Ser Add Ent |
Research reporting series. Environmental monitoring. |
| Alternate Title |
One step method for the determination of carbamate pesticides by derivatization with alpha-bromo-2,3,4,5,6-pentafluorotoluene |
| NTIS Title Notes |
Final rept.. |
| PUB Date Free Form |
1979 |
| Series Title Traced |
Research reporting series. |
| Series Title Untraced |
Research reporting series. 4, Environmental monitoring. |
| Category Codes |
6F; 7D; 68E; 57P; 99A |
| NTIS Prices |
PC A06/MF A01 |
| Primary Description |
600/11 |
| BIB Level |
m |
| Medium |
unmediated |
| Content |
text |
| Carrier |
volume |
| Cataloging Source |
OCLC/T |
| Control Number |
323775018 |
| OCLC Time Stamp |
20180717120107 |
| Language |
eng |
| Origin |
OCLC |
| Type |
MERGE |
| OCLC Rec Leader |
02163cam 2200457Ka 45010 |
