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Main Title Polysiloxane Deactivated Fused Silica Capillaries Containing Immobilized Stationary Phases.
Author Moseley, M. A. ; Pellizzari, E. D. ;
CORP Author Research Triangle Inst., Research Triangle Park, NC.;Environmental Research Lab.-Duluth, MN.
Year Published 1982
Report Number EPA-R-807167; EPA-600/J-82-370;
Stock Number PB83-239798
Additional Subjects Silicon dioxide ; Stationary processes ; Catalysis ; Deactivation ; Adsorption ; Capillaries ; Gas chromatography ; Reprints ; Polysiloxane
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NTIS  PB83-239798 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 7p
Abstract This article describes a method of preparing immobilized stationary phases which has arisen from the author's work on polysiloxane deactivation of fused silica capillaries. Although acid treatment is often omitted with fused silica capillaries, there are good reasons for hydrothermal treatment of this column material. Use of Grob's peroxide method gave immobilized 0.25 micrometers films of SE-54; lowering of the immobilization temperature permitted immobilization of 0.1 micrometers films of the same phase.
Availability Notes Pub. in Jnl. of High Resolution Chromatography and Chromatography Communications 5, p472-475 1982.
NTIS Title Notes Journal article.
Title Annotations Reprint: Polysiloxane Deactivated Fused Silica Capillaries Containing Immobilized Stationary Phases.
PUB Date Free Form c1982
Category Codes 7D; 99A
NTIS Prices Not available NTIS
Primary Description 600/03
Document Type NT
Cataloging Source NTIS/MT
Control Number 332920111
Origin NTIS
Type CAT