| Main Title |
Measurement of polycyclic aromatic hydrocarbons in soils and sediments by partical-beam/high-performance liquid chromatography/mass spectrometry / |
| Author |
Pace, Chris M. ;
Miller, D. A. ;
Roby, M. R.
|
| Other Authors |
|
| CORP Author |
Lockheed Engineering and Sciences Co., Inc., Las Vegas, NV. Environmental Programs Office.;Environmental Monitoring Systems Lab., Las Vegas, NV. |
| Publisher |
U.S. Environmental Protection Agency, Office of Research and Development, Environmental Monitoring Systems Laboratory ; Distributed by the National Technical Information Service, |
| Year Published |
1992 |
| Report Number |
EPA 600-4-91-032; 68-C0-0049; EPA-68-CO-0049; PB92188721 |
| Stock Number |
PB92-188721 |
| OCLC Number |
37429561 |
| Subjects |
Chromatographic analysis
|
| Additional Subjects |
Aromatic polycyclic hydrocarbons ;
Liquid chromatography ;
Mass spectroscopy ;
Soils ;
Sediments ;
Graphs(Charts) ;
Toxic substances
|
| Internet Access |
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| ELBD ARCHIVE |
EPA 600-4-91-032 |
Received from HQ |
AWBERC Library/Cincinnati,OH |
10/04/2023 |
| NTIS |
PB92-188721 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
viii, 18, [23] pages ; 28 cm |
| Abstract |
An analytical method was developed for the measurement of certain polycyclic aromatic hydrocarbons (PAHs) in soils and sediments by particle beam liquid chromatography/mass spectrometry. The method applies to PAHs with a molecular weight greater than 220. Samples are prepared by SW-846 Method 3540 with optional cleanup using SW-846 Method 3630. The sample extracts are then analyzed for PAHs using a particle beam liquid chromatography/mass spectrometry system. Method detection limits are within the range of 0.01 - 0.10 microg/g depending on the sample size. Mean method accuracy was greater than 75 percent for most of the target analytes with relative standard deviation values between 10 percent to 20 percent. An analysis of a standard reference material using this method agreed with certified values and with an analysis performed using high performance liquid chromatography (HPLC) with fluorescence detection (SW-846 Method 8310). The method shows potential as a means to measure high molecular weight PAHs not measured by current EPA methods. |
| Notes |
"EPA 600-4-91-032." "May 1992." Cover title. "EPA Contract No. 68-03-3249." "Technical monitor, L.D. Betowski." Includes bibliographical references. |
| Place Published |
Las Vegas, Nev. Springfield, Va. |
| Supplementary Notes |
Sponsored by Environmental Monitoring Systems Lab., Las Vegas, NV. |
| Corporate Au Added Ent |
Lockheed Engineering & Sciences Company.; Environmental Monitoring Systems Laboratory (Las Vegas, Nev.); United States. Environmental Protection Agency. Office of Research and Development. |
| PUB Date Free Form |
1992 |
| NTIS Prices |
PC A03/MF A01 |
| BIB Level |
m |
| Medium |
unmediated |
| Content |
text |
| Carrier |
volume |
| Cataloging Source |
OCLC/T |
| OCLC Time Stamp |
20180409054522 |
| Language |
eng |
| Origin |
OCLC |
| Type |
MERGE |
| OCLC Rec Leader |
01828cam 2200433Ka 45010 |
