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Main Title Developments in the Supercritical Fluid Extraction of Chlorophenoxy Acid Herbicides from Soil Samples.
Author Lopez-Avila, V. ; Dodhiwala, N. S. ; Beckert, W. F. ;
CORP Author Midwest Research Inst., Mountain View, CA. California Operations.;Environmental Monitoring Systems Lab., Las Vegas, NV.
Publisher c1993
Year Published 1993
Report Number EPA-68-C1-0029; EPA/600/J-94/268;
Stock Number PB94-182326
Additional Subjects Herbicides ; Soil pollution ; Extraction ; Reprints ; Supercritical flow ; Carbon dioxide ; Pollution monitoring ; Remedial action ; Sampling ; EPA SW-846 Method 8151 ; In situ treatment ; Chlorophenoxy acid herbicides
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NTIS  PB94-182326 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 9p
Abstract Extraction of chlorophenoxy acid herbicides from soil samples with supercritical carbon dioxide as extractant and tetrabutylammonium hydroxide and methyl iodide as derivatization agents was investigated. The extraction was carried out at 400 atm and 80 degrees C for 15 min static, followed by 15 min dynamic, at a carbon dioxide flow rate of approximately 1.5 mL/min (as liquid). The use of other derivatization agents (trimethylphenylammonium hydroxide, benzyltrimethylammonium chloride, and benzyltriethylammonium chloride) proved to be less effective than the tetrabutylammonium hydroxide/methyl iodide combination. (Copyright (c) 1993 American Chemical Society.)
Supplementary Notes Pub. in Jnl. of Agricultural and Food Chemistry, v41 n1 p2038-2044 1993. Sponsored by Environmental Monitoring Systems Lab., Las Vegas, NV.
NTIS Title Notes Journal article.
Title Annotations Reprint: Developments in the Supercritical Fluid Extraction of Chlorophenoxy Acid Herbicides from Soil Samples.
Category Codes 68E; 99B
NTIS Prices PC A02/MF A01
Primary Description 600/07
Document Type NT
Cataloging Source NTIS/MT
Control Number 421724799
Origin NTIS
Type CAT