| Main Title |
GC-MS (Gas Chromatographic-Mass Spectrometric) Suitability Testing of RCRA Appendix VIII and Michigan List Analytes. |
| Author |
Lucas, S. V. ;
Kornfeld, R. A. ;
|
| CORP Author |
Battelle Columbus Labs., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH. |
| Year Published |
1987 |
| Report Number |
EPA-68-03-3224; EPA/600/4-87/024; |
| Stock Number |
PB87-227674 |
| Additional Subjects |
Chemical analysis ;
Hazardous materials ;
Solid waste disposal ;
Gas chromatography ;
Mass spectrometry ;
Soil analysis ;
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| NTIS |
PB87-227674 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
79p |
| Abstract |
As a first step in a hierarchical scheme to demonstrate the suitability of present U.S. Environmental Protection Agency (USEPA) analysis methods and/or develop new methodology, the gas chromatographic (GC) separation and mass spectrometric (MS) detection characteristics of 328 toxic and/or hazardous organic materials have been investigated. Volatile and semivolatile analytes were tested using the GC/MS conditions specified in the USEPA Methods 8240 and 8270, respectively, as modified by the Contractor Laboratory Program (CLP) protocol. Standard mixtures of analytes were analyzed by septum injection onto the analytical column without any prior sample work-up procedures. For the 187 analytes that proved suitable for GC/MS analysis by Methods 8240 and 8270, the relevant characteristics for GC retention (retention time and relative retention index) and for MS detection (recommended quantification ion and confirmation ions with relative abundances and response factor relative to the internal standard) are reported. For analytes not detected by GC/MS or not included, a priori, recommendations for future work are made. |
| Supplementary Notes |
Sponsored by Environmental Monitoring and Support Lab.-Cincinnati, OH. |
| NTIS Title Notes |
Final rept.. |
| PUB Date Free Form |
Aug 87 |
| Category Codes |
68C#; 68E; 99A# |
| NTIS Prices |
PC A05/MF A01 |
| Primary Description |
600/06 |
| Document Type |
NT |
| Cataloging Source |
NTIS/MT |
| Control Number |
732431338 |
| Origin |
NTIS |
| Type |
CAT |
