| Main Title |
Analysis of Hazardous Waste and Environmental Extracts by Capillary Gas Chromatography/Fourier Transform Infrared Spectrometry and Capillary Gas Chromatography/Mass Spectrometry. |
| Author |
Gurka, D. F. ;
Hiatt, M. ;
Titus, R. ;
|
| CORP Author |
Environmental Monitoring Systems Lab., Las Vegas, NV. ;Nevada Univ., Las Vegas. |
| Year Published |
1984 |
| Report Number |
EPA/600/J-84/286; |
| Stock Number |
PB85-198380 |
| Additional Subjects |
Hazardous materials ;
Environmental surveys ;
Extraction ;
Chemical analysis ;
Comparison ;
Gas chromatography ;
Infrared spectroscopy ;
Mass spectroscopy ;
Sampling ;
Reprints ;
Fused silica capillary column gas chromatography ;
Fourier transform spectroscopy
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| NTIS |
PB85-198380 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
11p |
| Abstract |
The relative sensitivities of fused-silica capillary column gas chromatography/Fourier transform infrared spectrometry (FSCC/GC/FT-IR) versus packed-column GC/FT-IR and FSCC/GC/FT-IR versus fused-silica capillary column gas chromatography/mass spectrometry (FSCC/GC/MS) were compared. As part of this study, complex environmental extracts were analyzed by both FSCC/GC/FT-IR and FSCC/GC/MS. The on-line library search results for both techniques were compared with the visually-checked spectral results for all FSCC/GC/FT-IR detectable analytes. Positive analyte identification depended strongly on sample preparation technique, search library content, chromatographic resolution and compound class. It was concluded that a target compound approach would not have utilized much of the available analyte information in these extracts. |
| Supplementary Notes |
Prepared in cooperation with Nevada Univ., Las Vegas. |
| Availability Notes |
Pub. in Analytical Chemistry 56, n7 p1102-1110 Jun 84. |
| NTIS Title Notes |
Journal article. |
| Title Annotations |
Reprint: Analysis of Hazardous Waste and Environmental Extracts by Capillary Gas Chromatography/Fourier Transform Infrared Spectrometry and Capillary Gas Chromatography/Mass Spectrometry. |
| PUB Date Free Form |
c1984 |
| Category Codes |
7D; 68; 99A |
| NTIS Prices |
Not available NTIS |
| Primary Description |
600/07 |
| Document Type |
NT |
| Cataloging Source |
NTIS/MT |
| Control Number |
519925519 |
| Origin |
NTIS |
| Type |
CAT |
