| Main Title |
Determination of Pentachlorophenol in Blood, Urine, Tissue, and Clothing. |
| Author |
Barthel, W. F. ;
Curley, August ;
Thrasher, C. L. ;
Sedlak, V. A. ;
Armstrong., Robert ;
|
| CORP Author |
National Communicable Disease Center, Atlanta, Ga. |
| Year Published |
1968 |
| Stock Number |
PB-276 899, PB-276 897 |
| Additional Subjects |
Chemical analysis ;
Chlorine organic compounds ;
Blood analysis ;
Urine ;
Tissues(Biology) ;
Clothing ;
Electron capture ;
Gas chromatography ;
Mass spectroscopy ;
Thin layer chromatography ;
Fungus resistant coatings ;
Reprints ;
Phenol/pentachloro ;
Electron capture gas chromatography
|
| Holdings |
| Library |
Call Number |
Additional Info |
Location |
Last
Modified |
Checkout
Status |
| NTIS |
PB-276 899 |
Some EPA libraries have a fiche copy filed under the call number shown. |
|
07/26/2022 |
|
| Collation |
6p |
| Abstract |
An epidemic with two deaths occurred in a nursery in St. Louis after the use of pentachlorophenol as a mildew preventive with the laundry detergent. Samples of blood, urine, tissue, and clothing from the nursery were extracted with ethyl ether. The ether solution was extracted with 5% sodium hydroxide; the basic solution was acidified and then extracted with benzene. The benzene solution was analyzed by electron capture gas chromatography, using a 3% diethylene glycol succinate column with 2% sirupy phosphoric acid on 60-80 mesh Chromosorb G. Pentachlorophenol was found in the samples in sufficient quantity to account for the epidemic. The presence of pentachlorophenol was confirmed by gas chromatography-mass spectroscopy and by thin layer analysis. |
| Notes |
found in PB-276 897 titled: Journal articles on pesticide chemical analysis. Group 5. |
| Supplementary Notes |
Pub. in Jnl. of the Association of Official Analytical Chemists, v52 n2 p294-298, Mar 69. |
| Availability Notes |
Included in the report, Journal Articles on Pesticide Chemical Analysis. Group 5, PB-276 897. |
| Title Annotations |
Reprint: Determination of Pentachlorophenol in Blood, Urine, Tissue, and Clothing, |
| PUB Date Free Form |
4 Sep 68 |
| Category Codes |
7D; 6E; 99A; 57D |
| NTIS Prices |
(Order as PB-276 897, MF A01) |
| Primary Description |
500/01 |
| Document Type |
NT |
| Cataloging Source |
NTIS/MT |
| Control Number |
323732617 |
| Origin |
NTIS |
| Type |
CAT |
