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Main Title Determination of Phenolic Compounds in Alternate Fuel Matrices.
Author Guenther, F. R. ; Parris, R. M. ; Chesler, S. N. ; Hilpert, L. R. ;
CORP Author National Bureau of Standards, Washington, DC.;Department of Energy, Washington, DC.;Environmental Protection Agency, Washington, DC.
Year Published 1981
Stock Number PB81-199176
Additional Subjects Phenols ; Chemical analysis ; Shale oil ; Extraction ; Gas chromatography ; Separated ; Mass spectroscopy ; Reprints ; Solvent refined coal ; NTISCOMNBS ; NTISDE ; NTISEPAG
Library Call Number Additional Info Location Last
NTIS  PB81-199176 Some EPA libraries have a fiche copy filed under the call number shown. 07/26/2022
Collation 6p
Abstract The gas-chromatographic determination of underivatized, methyl substituted phenols in shale oil and solvent refined coal is described. A simple acid/base extraction procedure was followed by injection onto a 20 meter Pluronic L64 capillary column. Fourteen phenols were separated and identified including phenol, the cresols, and all the dimethyl phenols. Identification was done on a GC/MS equipped with a Pluronic L64 capillary column. Isomers were further verified by comparison of pure standard retention times. Quantitation was done utilizing an internal standard procedure. Quantitative data is given for seven phenols in the range of 168 microgram/g to 29100 microgram/g.
Supplementary Notes Sponsored in part by Department of Energy, Washington, DC., and Environmental Protection Agency, Washington, DC.
Availability Notes Pub. in Jnl. of Chromatography 207, p256-261 1981.
NTIS Title Notes Final rept..
Title Annotations Reprint: Determination of Phenolic Compounds in Alternate Fuel Matrices.
PUB Date Free Form 1981
Category Codes 21D; 7D; 97K; 99A; 86V
NTIS Prices Not available NTIS
Document Type NT
Cataloging Source NTIS/MT
Control Number 323798034
Origin NTIS
Type CAT