||Determination of Phenolic Compounds in Alternate Fuel Matrices.
Guenther, F. R. ;
Parris, R. M. ;
Chesler, S. N. ;
Hilpert, L. R. ;
||National Bureau of Standards, Washington, DC.;Department of Energy, Washington, DC.;Environmental Protection Agency, Washington, DC.
Chemical analysis ;
Shale oil ;
Gas chromatography ;
Mass spectroscopy ;
Solvent refined coal ;
||Some EPA libraries have a fiche copy filed under the call number shown.
||The gas-chromatographic determination of underivatized, methyl substituted phenols in shale oil and solvent refined coal is described. A simple acid/base extraction procedure was followed by injection onto a 20 meter Pluronic L64 capillary column. Fourteen phenols were separated and identified including phenol, the cresols, and all the dimethyl phenols. Identification was done on a GC/MS equipped with a Pluronic L64 capillary column. Isomers were further verified by comparison of pure standard retention times. Quantitation was done utilizing an internal standard procedure. Quantitative data is given for seven phenols in the range of 168 microgram/g to 29100 microgram/g.
||Sponsored in part by Department of Energy, Washington, DC., and Environmental Protection Agency, Washington, DC.
||Pub. in Jnl. of Chromatography 207, p256-261 1981.
|NTIS Title Notes
||Reprint: Determination of Phenolic Compounds in Alternate Fuel Matrices.
|PUB Date Free Form
||21D; 7D; 97K; 99A; 86V
||Not available NTIS