Record Display for the EPA National Library Catalog

RECORD NUMBER: 18 OF 77

OLS Field Name OLS Field Data
Main Title Evaluation of a microwave-induced plasma spectrometer : for trace analysis /
Author Seitz, William Rudolf.
CORP Author Environmental Protection Agency, Athens, Ga. Southeast Environmental Research Lab.
Publisher National Environmental Research Center, Office of Research and Development, U.S. Environmental Protection Agency,
Year Published 1974
Report Number EPA-660/2-73-009; EPA-ROAP-16ADN-32; 06841
Stock Number PB-231 390
OCLC Number 01275923
Subjects Spectrometer. ; Microwave spectroscopy. ; Trace elements--Analysis.
Additional Subjects Spectrochemical analysis ; Trace elements ; Water analysis ; Atomization ; Metals ; Microwaves ; Sensitivity ; Excitation ; Calibration ; Lead(Metal) ; Mercury ; Cadmium ; Arsenic ; Atomic spectroscopy ; Helium plasma ; Water pollution detection ; Microwave gas discharges
Internet Access
Description Access URL
http://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=200136D4.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EJAD  EPA 660/2-73-009 Region 3 Library/Philadelphia, PA 05/24/1996
EJBD ARCHIVE EPA 660-2-73-009 Headquarters Library/Washington,DC 05/20/2013
EJBD  EPA 660-2-73-009 c.1 Headquarters Library/Washington,DC 05/21/2013
EKAM  QC373.S7S453 Region 4 Library/Atlanta,GA 02/15/1997
ESBD  EPA-660-2-73-009 NHEERL/WED Library/Corvallis,OR 09/19/2017
NTIS  PB-231 390 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 01/01/1988
Collation iv, 19 pages ; 27 cm.
Abstract
A low pressure microwave-induced plasma in helium was evaluated as an excitation source for spectrochemical analysis of trace metals in water. The sample was introduced by evaporating a 5-microliter drop of solution on a wire filament and atomizing the solids by the discharge of a capacitor through the filament. The height of the resulting pulse from the photo detector was automatically recorded. Repeatability was about 10% and detection limits were 1 to 25 pg for As, Cd, Hg, and Pb. Slopes of calibration curves depended strongly on matrix and filament effects and the maximum solids loading of the filament was about 5 micrograms.
Notes
Includes bibliographical references (pages 17-19).