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RECORD NUMBER: 6 OF 20

OLS Field Name OLS Field Data
Main Title Preparation of the Components of the Modified Method 5 (Method 0010) Sampling Train for Analysis by SW-846 Method 8270.
Author McGaughey, J. F. ; Merrill, R. G. ; Bursey, J. T. ; Wagoner, D. E. ; Jackson, M. D. ;
CORP Author Radian Corp., Research Triangle Park, NC.;Environmental Protection Agency, Research Triangle Park, NC. Atmospheric Research and Exposure Assessment Lab.
Publisher Dec 93
Year Published 1993
Report Number EPA-68-D1-0010; EPA/600/A-94/098;
Stock Number PB94-176641
Additional Subjects Air pollution sampling ; Chemical analysis ; Halogenated hydrocarbons ; Field tests ; Boilers ; Stationary sources ; Emission factors ; Statistical analysis ; Analytical techniques ; Design criteria ; Test methods ; Sample preparation ; Precision ; Validation ; Bias ; Quality assurance ; Reprints ; EPA Method 5 ; EPA Method 0010 ; SW-846 Method 8270 ; SemiVOST(Semi-volatile Organic Sampling Train) ; Semivolatile organic compounds ; Clean Air Act Amendments of 1990
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
NTIS  PB94-176641 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 09/01/1994
Collation 13p
Abstract
In a field evaluation study for semivolatile halogenated organic compounds listed in Title III of the Clean Air Act Amendments of 1990, dynamic spiking experiments using a liquid solution were performed in the field. Two of four quadruple sampling trains were spiked for eight sampling runs. Method 0010 train components were prepared and analyzed in three parts: filter/front halt rinse, XAD-2 resin, and condensate/condensate rinse. Because the results were at variance with results obtained for analytes spiked in laboratory studies and a previous field study, the sample preparation process was investigated in detail. Sample preparation procedures had followed Method 0010, but use of some procedures which were not specifically prohibited by Method 0010 had depressed compound recoveries. To ensure that the sample preparation procedures for Method 0010 train components were clear and unamibiguous, a new protocol to address preparation of Method 0010 train components for Method 8270 analysis was written.