Record Display for the EPA National Library Catalog

RECORD NUMBER: 1558 OF 1607

OLS Field Name OLS Field Data
Main Title USEPA (United States Environmental Protection Agency) Method Study 35.SW Method 3005. Acid Digestion of Waters for Total Recoverable or Dissolved Metals for Analyses by Flame Atomic Absorption Spectroscopy.
Author Edgell, K. W. ;
CORP Author Bionetics Corp., Cincinnati, OH.;Environmental Monitoring Systems Lab., Cincinnati, OH.
Publisher Apr 89
Year Published 1989
Report Number EPA-68-03-3254; EPA/600/4-89/015;
Stock Number PB89-190573
Additional Subjects Chemical analysis ; Ground water ; Hazardous materials ; Metals ; Site surveys ; Solid waste disposal ; Tables(Data) ; Concentration(Composition) ; Quality assurance ; Quality control ; Data processing ; Emission spectroscopy ; Atomic spectroscopy ; Water pollution detection ; Water pollution sampling
Holdings
Library Call Number Additional Info Location Last
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Status
NTIS  PB89-190573 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 08/24/1989
Collation 281p
Abstract
An interlaboratory collaborative study was conducted to determine the precision and bias (recovery) of Solid Waste (SW) Method 3005 for the analysis of 21 elements in ground water. The study design was based upon Youden's non-replicate plan for collaborative tests of analytical methods. Each water type was spiked with six concentrations (as three Youden pairs) of the 21 test elements and was prepared using nitric/hydrochloric acid digestion and analyzed by Atomic Absorption (AA-Direct Aspiration). Test data from three spiked ground water sources were compared against reagent water which was used as a control. The study produced, for each element, measures of precision and mean recovery for the acid digestion/AA-Direct Aspiration and compared the performance of the method between water types and reagent water.