Record Display for the EPA National Library Catalog

RECORD NUMBER: 45 OF 67

OLS Field Name OLS Field Data
Main Title Methodology for measurement of polychlorinated biphenyls in ambient air and stationary sources - a review /
Author Margeson, John H.
CORP Author Environmental Monitoring and Support Lab., Research Triangle Park, N.C. Quality Assurance Branch.
Publisher U.S. Environmental Protection Agency,
Year Published 1976
Report Number EPA-600/4-77-021
Stock Number PB-269 350
OCLC Number 09519782
Subjects Polychlorinated biphenyls--Measurement. ; Air--Pollution--Measurement.
Additional Subjects Reviews ; Chlorine organic compounds ; Sampling ; Gas analysis ; Chemical analysis ; Monitoring ; Air pollution ; Polyurethane resins ; Foams ; Extraction ; Gas chromatography ; Electron capture ; Absorption ; Concentration(Composition) ; Physical properties ; Chemical properties ; Stationary sources ; Polychlorinated biphenyls ; Air pollution detection ; Aroclors ; Electron capture detectors ; Biphenyl/chloro
Internet Access
Description Access URL
https://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=9101A4CU.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EJAD  EPA 600/4-77-021 Region 3 Library/Philadelphia, PA 01/28/2000
EJBD ARCHIVE EPA 600-4-77-021 Headquarters Library/Washington,DC 05/06/2014
EJED  EPA 600/4-77-021 OCSPP Chemical Library/Washington,DC 06/16/1989
EKAM  EPA-600/4-77-021 Region 4 Library/Atlanta,GA 05/27/1994
EKBD  EPA-600/4-77-021 Research Triangle Park Library/RTP, NC 07/25/2003
ELDD  EPA-600/4-77-021 NHEERL/MED Library/Duluth,MN 03/13/1999
ESAD  EPA 600-4-77-021 Region 10 Library/Seattle,WA 03/23/2010
NTIS  PB-269 350 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 07/22/2019
Collation vi, 31 pages : charts ; 28 cm.
Abstract
The state of development of methodology for measurement of polychlorinated biphenyls (PCBs) in ambient air and stationary sources was reviewed. The most promising method for ambient air measurements involves collection of PCBs on polyurethane foam, extraction with an organic solvent, removal of interferences by colum chromatography, and confirmation and analysis by electron-capture gas chromatography. Quantitation by perchlorination of PCBs to decachlorobipheny (DCB) is the most promising quantitation technique, but the procedure has not yet been perfected to the points are quantitatively converted to DCB. Perfection of this technique should allow for significant improvement in the quality of ambient PCB data being generated. Source and ambient methods differ mainly in sampling. Work on methodology for stationary sources is in the early stages of development and futher investigations are needed. The report contains 56 references.
Notes
References included.
Contents Notes
The state of development of methodology for measurement of polychlorinated biphenyls (PCBs) in ambient air and stationary sources was reviewed. The most promising method for ambient air measurements involves collection of PCBs on polyurethane foam, extraction with an organic solvent, removal of interferences by column chromatography, and confirmation and analysis by electron-capture gas chromatography. Quantitation by perchlorination of PCBs to decachlorobiphenyl (DCB) is the most promising quantiation technique, but the procedure has not yet been perfected to the point where all PCBs are quantitatively converted to DCB. Perfection of this technique should allow for significant improvement in the quality of ambient PCB data being generated. Source and ambient methods differ mainly in sampling. Work on methodology for stationary sources is in the early stages of development and further investigations are needed.