Record Display for the EPA National Library Catalog

RECORD NUMBER: 7 OF 7

OLS Field Name OLS Field Data
Main Title Single Laboratory Validation of EPA (Environmental Protection Agency) Method 8030: Acrolein, Acrylonitrile, and Acetonitrile.
Author Lucas, S. V. ; Cole, T. F. ; Riggin, A. ; Cooke, W. M. ;
CORP Author Battelle Columbus Labs., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH.
Year Published 1985
Report Number EPA-68-03-1760; EPA/600/4-85/010;
Stock Number PB85-165827
Additional Subjects Chromatographic analysis ; Acroleins ; Acrylonitriles ; Acetonitrile ; Environmental surveys ; Ground water ; Water analysis ; Chemical analysis ; Performance evaluation ; Revisions ; EPA method 8030 ; Water pollution detection ; Solid wastes ; Liquid wastes ; Purge and trap method
Holdings
Library Call Number Additional Info Location Last
Modified
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Status
NTIS  PB85-165827 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/21/1988
Collation 152p
Abstract
USEPA Method 8030 was modified and evaluated with revised chromatographic conditions for the determination of acrolein, acrylonitrile, and acetonitrile in groundwater, solid, and organic liquid matrices. Groundwater was analyzed by the heated purge-and-trap method; a solid waste was analyzed by the polyethylene glycol (PEG) heated purge-and-trap technique and by the heated headspace method; and a liquid organic waste was analyzed by direct liquid injection and by the heated headspace method. The manual heated headspace method gave distinctly less accurate and less precise results than the PEG/purge-and-trap method for the determination of acetonitrile and acrylonitrile in the solid waste sample. Acrolein was not recovered at all by the method. The headspace method gave extremely erratic results for the analysis of the organic liquid waste.