Record Display for the EPA National Library Catalog

RECORD NUMBER: 3 OF 7

OLS Field Name OLS Field Data
Main Title Evaluation of Methods for Hazardous Chemicals Listed in Appendix D to 40 CFR 122 (Table 5).
Author Cole, T. F. ; Lucas, S. V. ; Cooke, W. M. ;
CORP Author Battelle Columbus Div., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH.
Year Published 1985
Report Number EPA-68-03-1760; EPA/600/4-86/001;
Stock Number PB86-136520
Additional Subjects Hazardous materials ; Chemical compounds ; Water analysis ; Tables(Data) ; Performance evaluation ; Chromatographic analysis ; Extraction ; Revisions ; Chemical analysis ; Water pollution detection ; Purge and trap techniques ; Procedures
Holdings
Library Call Number Additional Info Location Last
Modified
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Status
NTIS  PB86-136520 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/21/1988
Collation 123p
Abstract
Of 75 organic compounds listed in Appendix D to 40 CRF 122 (Table V), 24 compounds have not been previously shown amenable to existing EPA Methods for analysis in water and wastewater. The present work reports on 17 of those 24 compounds using 600 Methods with appropriate modification. The approach was to demonstrate performance in the areas: (1) chromatography - using fused silica capillary columns, (2) extraction and concentration, and (3) cleanup. When attempts were successful, the integrated method was tested for accuracy and precision. A purge-and-trap approach was shown to have substantial problems with the volatile amines. An automated heated headspace/capillary column method worked poorly for monoalkyl amines. A specially prepared column packing was effective for all of the volatile amines. No method development was achieved for either ethanolamine or isopropanolamine.