Record Display for the EPA National Library Catalog

RECORD NUMBER: 106 OF 2557

OLS Field Name OLS Field Data
Main Title An intercomparison of grinding techniques used for the preparation of lead-in paint samples /
Author Hodson, L. L. ; Hardison, E. D. ; Leinbach, A. A. ; Messner, M. J. ; Binstock, D. A.
Other Authors
Author Title of a Work
Hardison, E. D.
Harper, S. L.
Leinbach, A. A.
Messner, M. J.
Binstock, D. A.
Gutknecht, W. F.
CORP Author Research Triangle Inst., Research Triangle Park, NC. Center for Environmental Measurements and Quality Assurance.;Environmental Protection Agency, Research Triangle Park, NC. National Exposure Research Lab.
Publisher U.S. Environmental Protection Agency, Office of Research and Development, National Exposure Research Laboratory,
Year Published 1997
Report Number EPA/600/R-95/112; EPA-68-D1-0009; EPA-68-D5-0040; RTI-91U-6660-014; RTI-91U-6970-255
Stock Number PB98-131881
OCLC Number 47694691
Additional Subjects Lead(Metal) ; Paints ; Grinding ; Sample preparation ; Sampling ; Chemical analysis ; Comparative evaluations ; Statistical analysis ; Quality assurance ; Quality control
Internet Access
Description Access URL
http://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=9100CG7U.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EJED  EPA/600/R-95/112 OCSPP Chemical Library/Washington,DC 10/04/2002
NTIS  PB98-131881 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 01/01/1988
Collation 88 pages ; 28 cm
Abstract
The method used to grind a dried paint sample prior to acid digestion and measurement (by inductively coupled plasma (ICP) emission spectrometry or some other means), may affect the recovery of lead from the paint. In the study, five grinding techniques were compared. These were: (1) grinding with a glass rod at room temperature in a 50-mL centrifuge tube, (2) grinding with a glass rod at dry ice temperature in a 50-mL centrifuge tube, (3) grinding with a mortar and pestile, (4) grinding with a motorized blender, and (5) grinding with a cryogenic mill that operated at liquid nitrogen temperature.
Notes
"S.L. Harper, work assignment manager." "EPA/600/R-95/112." ""September 1997." Microfiche.