Record Display for the EPA National Library Catalog

RECORD NUMBER: 27 OF 82

OLS Field Name OLS Field Data
Main Title EPA (Environmental Protection Agency) Method Study 19, Method 609 (Nitroaromatics and Isophorone).
Author Kinzer, G. ; Riggin, R. ; Bishop, T. ; Birts, M. A. ; Howard, C. C. ;
CORP Author Battelle Columbus Labs., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH.
Year Published 1984
Report Number EPA-68-03-2624; EPA-600/4-84-018;
Stock Number PB84-176908
Additional Subjects Nitrobenzenes ; Water analysis ; Solvent extraction ; Chemical analysis ; Water pollution ; Concentration(Composition) ; Gas chromatography ; Water pollution ; Nitrogen organic compounds ; EPA method 609 ; Isophorone ; Toluene/dinitro ; Water pollution detection ; Electron capture spectroscopy ; Flame ionization spectroscopy
Holdings
Library Call Number Additional Info Location Last
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Status
NTIS  PB84-176908 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. 06/23/1988
Collation 77p
Abstract
An interlaboratory study in which 18 laboratories participated was conducted to provide precision and accuracy statements for the proposed EPA Method 609 for measuring concentrations of the Category 4 chemicals nitrobenzene, isophorone, 2,4-dinitrotoluene and 2,6-dinitrotoluene in municipal and industrial aqueous discharges. Method 609 involves solvent extraction of the pollutants with methylene chloride followed by Florisil clean-up and subsequent gas chromatographic analysis of the four subject compounds using flame ionization and electron capture detection techniques. The study design was based on Youden's plan for collaborative tests of analytical methods. Three Youden pair samples of the test compounds were spiked into six types of test waters and then analyzed. The test waters were distilled water, tap water, a surface water, and three different industrial wastewater effluents. The resulting data were statistically analyzed using the computer program entitled 'Interlaboratory Method Validation Study' (IMVS).