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RECORD NUMBER: 355 OF 467

OLS Field Name OLS Field Data
Main Title Sensitizing the 4-Aminoantipyrine Reaction with Phenolic Materials for use in Water and Waste Analysis.
Author Ettinge, M. B. ; Ruchhof, C. C. ; Lishk, R. J. ;
CORP Author Environmental Health Center, Cincinnati, Ohio.
Year Published 1950
Stock Number PB-216 759
Additional Subjects ( Water analysis ; Phenols) ; ( Colorimetric analysis ; Phenols) ; ( Spectroscopic analysis ; Phensols) ; Dyes ; Antipyrine/amino ; Water pollution detection
Holdings
Library Call Number Additional Info Location Last
Modified
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Status
NTIS  PB-216 759 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/23/1988
Collation 38p
Abstract
The use of 4-aminoantipyrine was proposed by Emerson in a new color test for phenols. As outlined by Emerson, the essentials of the reaction consist of bringing together the phenolic material, the 4-aminoantipyrine and an alkaline oxidant in a solution of sufficiently high pH to prevent the formation of antipyrine red. Potassium ferricyanide was recommended as the oxidant. The work to be described has had two goals: Evaluation of the reaction variables which affect usage of Emerson's reagent for the determination of the simpler phenols; and Devising a procedure sufficiently sensitive to detect a one p.p.b. concentration of phenol.