Record Display for the EPA National Library Catalog

RECORD NUMBER: 46 OF 56

OLS Field Name OLS Field Data
Main Title Sampling and analysis of reduced and oxidized species in process streams : final report /
Author Maddalone, R. F. ; Scinto, L. L. ; Yamada, M. M.
Other Authors
Author Title of a Work
Scinto, L. L.
Yamada, M. M.
CORP Author TRW Defense and Space Systems Group, Redondo Beach, CA.;Industrial Environmental Research Lab., Research Triangle Park, NC.
Publisher U.S. Environmental Protection Agency, Industrial Environmental Research Laboratory ; National Technical Information Service [distributor],
Year Published 1979
Report Number EPA-600/2-79-201
Stock Number PB80-191281
OCLC Number 08398264
Subjects Flue gases--Desulfurization--Environmental aspects. ; Coal--Desulfurization--Environmental aspects. ; Flue gases--Desulphurization--Environmental aspects ; Coal--Desulphurization--Environmental aspects
Additional Subjects Gas analysis ; Chemical analysis ; Air pollution ; Sampling ; Inorganic compounds ; Industrial wastes ; Combustion products ; X ray diffraction ; Infrared spectroscopy ; Thermal analysis ; Electrochemistry ; Oxidation ; Reduction ; Air pollution detection ; Flue gas desulfurization ; Ion chromatography
Internet Access
Description Access URL
http://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=91018EWB.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EHAM  TD172.E46 1979 Region 1 Library/Boston,MA 04/29/2016
EJAD  EPA 600/2-79-201 Region 3 Library/Philadelphia, PA 06/16/2000
EKAM  600/2-79/201 Region 4 Library/Atlanta,GA 09/24/1999
EKBD  EPA-600/2-79-201 Research Triangle Park Library/RTP, NC 07/04/2003
ERAD  EPA 600/2-79-201 Region 9 Library/San Francisco,CA 10/01/2012
ESAD  EPA 600-2-79-201 Region 10 Library/Seattle,WA 03/23/2010
NTIS  PB80-191281 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/23/1988
Collation vi, 218 pages : illustrations ; 28 cm.
Abstract
The report gives results of a program of over 60 tasks involving the evaluation, development, testing, and field adaptation of measurement techniques for elemental analysis and inorganic compound identification in process and effluent streams. Procedures for particulate sampling at the inlet and outlet of FGD systems were developed. Methods for H2SO4 sampling in flue gas streams were developed based on the controlled condensation of H2SO4 vapor (a manual procedure was used as the basis for an automated H2SO4 monitoring instrument that was built and tested). Two procedure manuals were written for reduced and oxidized inorganic species. The reduced species manual detailed GC and GC/MS procedures for identifying organometallic compounds as well as homologous series such as RSH and RNH. The oxidized species were identified using an integrated series of analytical methods such as AAS, ICAP, XRD, FTIR, ESCA, and SEM-EDX. The procedures developed, applied to samples from several EPA programs, showed that the analysis scheme is applicable to most solid samples from combustion sources. Ion chromatographic procedures were also developed for analyzing FGD system slurry streams. The use of pH and chloride electrodes for controlling FGD systems was investigated. The methodology for coal flow monitors was reviewed.
Notes
"TRW Defense and Space Systems Group." "November 1979." Includes bibliographical references. "Contract no. 68-02-2165, task no. 221, program element no. INE624."