Record Display for the EPA National Library Catalog

RECORD NUMBER: 25 OF 66

OLS Field Name OLS Field Data
Main Title Determination of Pentachlorophenol in Blood, Urine, Tissue, and Clothing.
Author Barthel, W. F. ; Curley, August ; Thrasher, C. L. ; Sedlak, V. A. ; Armstrong., Robert ;
CORP Author National Communicable Disease Center, Atlanta, Ga.
Year Published 1968
Stock Number PB-276 899, PB-276 897
Additional Subjects Chemical analysis ; Chlorine organic compounds ; Blood analysis ; Urine ; Tissues(Biology) ; Clothing ; Electron capture ; Gas chromatography ; Mass spectroscopy ; Thin layer chromatography ; Fungus resistant coatings ; Reprints ; Phenol/pentachloro ; Electron capture gas chromatography
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
NTIS  PB-276 899 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/23/1988
Collation 6p
Abstract
An epidemic with two deaths occurred in a nursery in St. Louis after the use of pentachlorophenol as a mildew preventive with the laundry detergent. Samples of blood, urine, tissue, and clothing from the nursery were extracted with ethyl ether. The ether solution was extracted with 5% sodium hydroxide; the basic solution was acidified and then extracted with benzene. The benzene solution was analyzed by electron capture gas chromatography, using a 3% diethylene glycol succinate column with 2% sirupy phosphoric acid on 60-80 mesh Chromosorb G. Pentachlorophenol was found in the samples in sufficient quantity to account for the epidemic. The presence of pentachlorophenol was confirmed by gas chromatography-mass spectroscopy and by thin layer analysis.
Notes
found in PB-276 897 titled: Journal articles on pesticide chemical analysis. Group 5.