Record Display for the EPA National Library Catalog

RECORD NUMBER: 37 OF 75

OLS Field Name OLS Field Data
Main Title EPA (Environmental Protection Agency) Method Study 26, Method 613, 2,3,7,8-Tetrachlorodibenzo-p-Dioxin.
Author Hileman, F. D. ; Kirk, D. E. ; Mazer, T. ; Synder, A. D. ; Warner, B. J. ;
CORP Author Monsanto Research Corp., Dayton, OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH.
Year Published 1984
Report Number EPA-68-03-2856; EPA-600/4-84-037;
Stock Number PB84-188879
Additional Subjects Water analysis ; Chlorine organic compounds ; Water pollution ; Pesticides ; Chemical analysis ; Performance evaluation ; Samples ; Laboratories ; Chromatographic analysis ; EPA method 613 ; Dioxin(Herbicide) ; Water pollution detection
Internet Access
Description Access URL
https://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=P100N9GW.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
NTIS  PB84-188879 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/23/1988
Collation 82p
Abstract
The experimental design and results of an interlaboratory study for dioxin in water is described herein. The interlaboratory study of EPA Method 613 consisted of the replicate analyses of a performance evaluation sample used primarily for determining laboratory competence and subsequent analyses of six sample concentrations and a blank in six different waters (42 samples). Statistical analyses and conclusions in this report are based on analytical data obtained by eleven collaborating laboratories. Participating laboratories were selected based upon technical evaluation of proposals and upon the analytical results of the prestudy samples. Data obtained from the interlaboratory study were analyzed employing US EPA's series of computer programs known as the Interlaboratory Method Validation Study (IMVS) system, which implements the concepts recommended in ASTM Standard D 2777. The statistical analyses included tests for the rejection of outliers, estimation of mean recovery (accuracy), estimation of single-analyst and overall precisions, and tests for the effect of water type on accuracy and precision.