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RECORD NUMBER: 24 OF 56

OLS Field Name OLS Field Data
Main Title Guidelines for the Determination of halogenated dibenzo-p-dioxins and dibenzojurans in commercial products /
Author Steele, David H. ; Steele, D. H. ; Stanley, J. S.
Other Authors
Author Title of a Work
Stanley, John S.
CORP Author Midwest Research Inst., Kansas City, MO.;Environmental Protection Agency, Washington, DC. Office of Pesticides and Toxic Substances.
Publisher U.S. Environmental Protection Agency,
Year Published 1987
Report Number EPA 560-5-87-007; MRI-8833-A01; EPA-68-02-4252
Stock Number PB88-199526
OCLC Number 862949349
Subjects Carcinogens. ; Chlorine compounds--Toxicology. ; Dibenzofurans--Toxicology. ; Dioxins--Toxicology.
Additional Subjects Hazardous materials ; Guidelines ; Mass spectrometry ; Halogen compounds ; Furans ; Chromatography ; Sampling ; Toxicology ; Toxic substances ; HDDs(Halogenated dibenzo-p-dioxins) ; HDFs(Halogenated dibenzofurans)
Internet Access
Description Access URL
http://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=9101VWN7.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EJBD ARCHIVE EPA 560-5-87-007 Headquarters Library/Washington,DC 11/18/2013
NTIS  PB88-199526 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 09/04/1988
Collation 126 pages : illustrations, charts ; 28 cm
Abstract
The determination of halogenated dibenzo-p-dioxins (HDDs) and dibenzofurans (HDFs) in commercial products require specific and sensitive analytical procedures. The development of methods for the measurement of HDD and HDF in commercial products is complicated by the diverse range of matrices, the potentially large number of halogenated (specifically chloro, bromo, or bromo/chloro) HDD and HDF congeners and potential interference due to major components of the product matrices. The report provides (1) a review of the literature pertaining to commercial product analyses for HDDs and HDFs, (2) detail on the total number of bromo, chloro, and bromo/chloro HDDs and HDFs, (3) a tentative scheme for the analysis of HDDs and HDFs in diverse matrices, and (4) guidelines for the high resolution gas chromatography/mass spectrometry or electron capture detector analysis of commercial products for HDDs and HDFs. The guidelines specify a rigorous QA/QC program for the analysis of the commercial products.
Notes
"EPA/560/5-87/007." Includes bibliographical references (pages A-83-A-88).
Contents Notes
The determination of halogenated dibenzo-p-diozins (HDDs) and dibenzofurans (HDFs) in commercial products require specific and sensitive analytical procedures. The development of methods for the measurement of HDD and HDF in commercial products is complicated by the diverse range of matrices, the potentially large number of halogenated (specifically chloro, bromo, or bromo/chloro) HDD and HDF congeners and potential interference due to major components of the product matrices. This report provides (1) a review of the literature pertaining to commercial product analyses for HDDs and HDFs, (2) detail on the total number of bromo, chloro, and bromo/chloro HDDs and HDFs, (3) a tentative scheme for the analysis of HDDs and HDFs in diverse matrices, and (4) guidelines for the high resolution gas chromatograchy/mass spectrometry or electron capture detector analysis of commercial products for HDDs and HDFs. The guidelines specify a rigorous QA/QC program for the analysis of the commercial products.