Record Display for the EPA National Library Catalog

RECORD NUMBER: 17 OF 26

OLS Field Name OLS Field Data
Main Title Manual of analytical quality control for pesticides and related compounds in human and environmental samples : a compendium of systematic procedures designed to assist in the prevention and control of analytical problems /
Author Sherma, Joseph.
Other Authors
Author Title of a Work
Beroza, Morton
Watts, Randall R.
CORP Author Lafayette Coll., Easton, PA. Dept. of Chemistry.;Environmental Protection Agency, Research Triangle Park, NC.
Publisher U.S. Environmental Protection Agency, Office of Research and Development, Health Effects Research Laboratory,
Year Published 1981
Report Number EPA-600/2-81-059; EPA-68-02-2474
Stock Number PB81-222721
OCLC Number 08299223
Subjects Pesticides.
Additional Subjects Pesticides ; Chemical analysis ; Quality control ; Manuals ; Sampling ; Gas chromatography ; Performance evaluation ; Thin layer chromatography ; Separation ; Urine ; Residues ; Carbamates ; Extraction ; Concentration(Composition) ; Extractions ; Phosphorus organic compounds ; High performance liquid chromatography ; Polychlorinated biphenyls
Internet Access
Description Access URL
http://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=30000EN6.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EMBD  PB81-222721 MF GWERD Library/Ada,OK 12/24/1992
NTIS  PB81-222721 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 01/01/1988
Edition Rev. 1981.
Collation x, 455 pages : illustrations ; 28 cm
Abstract
This manual provides the pesticide chemist with a systematic protocol for the quality control of analytical procedures and the problems that arise in the analysis of human or environmental media. It also serves as a guide to the latest and most reliable methodology available for the analysis of pesticide residues in these and other sample matrices. The sections dealing with inter- and intra-laboratory quality control, the evaluation and standardization of materials used, and the operation of the gas chromatograph are intended to highlight and provide advice in dealing with many problems which constantly plague the pesticide analytical chemist. Many aspects of the problem areas involved in extraction and isolation techniques for pesticides in various types of samples are discussed. Techniques for confirming the presence or absence of pesticides in sample materials are treated at some length. This highly important area provides validation of data obtained by the more routine analytical procedures. The gas chromatograph, being the principal instrument currently used in pesticide analysis, often requires simple servicing or troubleshooting. A section addressing some of these problems is included. Last, but by no means least in importance, is a short dissertation of the value and need for systematic training programs for pesticide chemists.
Notes
"Environmental Toxicology Division, Health Effects Research Laboratory." "April 1981." Includes bibliographical references. "Contract no. 68-02-2474." "EPA-600/2-81-059." "PB-81-222721." Microfiche.