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RECORD NUMBER: 1 OF 35

OLS Field Name OLS Field Data
Main Title Analytical procedures for aniline and selected derivatives in wastewater and sludge /
Author Riggin, Ralph M. ; Lucas, S. V. ; Cole, T. F. ; Birts, M. A.
Other Authors
Author Title of a Work
Cole, T. F.
Birts, M. A.
CORP Author Battelle Columbus Div., OH.;Environmental Monitoring and Support Lab.-Cincinnati, OH.
Publisher U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory,
Year Published 1984
Report Number EPA/600/4-84/009; EPA-68-03-2952
Stock Number PB84-140102
Subjects Lucas, S.V.
Additional Subjects Chemical analysis ; Waste water ; Water pollution ; Industrial wastes ; Gas chromatography ; Measuring instruments ; Mass spectroscopy ; Sludge ; Extraction ; Sewage sludge ; Water pollution detection ; High performance liquid chromatography ; EPA method 625 ; Solid wastes
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
NTIS  PB84-140102 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 01/01/1988
Collation 231 pages ; 28 cm
Abstract
This study involved the development and validation of analytical methods for determining aniline and 18 halogen and nitro-substituted derivatives in industrial wastewater and municipal sludge. Gas chromatography (GC) with a nitrogen-phosphorus detector (NPD) was found to be well suited as a determinative technique for anilines in wastewater. Detection limits of 1-5 micrograms/L were achieved using both packed and capillary columns. A GC-MS approach which was essentially the same as U.S. EPA Method 625 was found to be useful for identifying and determining anilines in industrial wastewater at the low micrograms/L level. A U.S. EPA Interim Method developed by EMSL-Cincinnati for the determination of priority pollutants in municipal sludge was evaluated and optimized for the determination of anilines. Detection limits of 50-300 micrograms/kg were achieved.
Notes
Caption title. "January 1984." "EPA-600/4-84-007." Microfiche.