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RECORD NUMBER: 12 OF 36

OLS Field Name OLS Field Data
Main Title Evaluation of Gel Permeation Chromatography for Clean Up of Human Adipose Tissue Samples for GC/MS Analysis of Pesticides and Other Chemicals.
Author MacLeod, Kathryn E. ; Hanisch, Robert C. ; Lewis, Robert G. ;
CORP Author Health Effects Research Lab., Research Triangle Park, NC.
Year Published 1981
Report Number EPA-600/J-82-005;
Stock Number PB82-246836
Additional Subjects Pesticides ; Chemical compounds ; Chemical analysis ; Tissues(Biology) ; Gas chromatography ; Mass spectroscopy ; Halogen organic compounds ; Humans ; Toxicology ; Reprints ; Gel permeation chromatography ; Polychlorinated biphenyls ; Polybrominated biphenyls ; Chlorinated napthalene
Holdings
Library Call Number Additional Info Location Last
Modified
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Status
NTIS  PB82-246836 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. 06/23/1988
Collation 5p
Abstract
Gel permeation chromatography (GPC) has been evaluated for clean up of human adipose tissue sample extracts in preparation for confirmatory analysis by gas chromatography-mass spectrometry (GC/MS). Studies were conducted with standard solutions, fortified chicken fat, and actual human adipose tissue samples. Nearly quantitative removal of lipid material was achieved with minimal losses of 16 organochlorine pesticides and metabolites: two polychlorinated biphenyl (PCB) mixtures, two chlorinated napthalene (PCN) mixtures, and a polybrominated biphenyl (PBB) mixture. Mass spectra free from interferences were obtained over the mass range from 46 m/z to 560 m/z.