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RECORD NUMBER: 1 OF 2

OLS Field Name OLS Field Data
Main Title Analysis and GC-MS characterization of toxaphene in fish and water /
Author Stalling, David L. ; Huckins., James N.
Other Authors
Author Title of a Work
Huckins, James N.,
CORP Author Fish and Wildlife Service, Columbia, Mo. Fish-Pesticide Research Lab.;Environmental Research Lab., Duluth, Minn.
Publisher U.S. Environmental Protection Agency, Office of Research and Development, Environmental Research Laboratory ; For sale by the National Technical Information Service,
Year Published 1976
Report Number EPA-600/3-76-076
Stock Number PB-257 773
OCLC Number 02487354
ISBN pbk.
Subjects Chromatographic analysis. ; Mass spectrometry. ; Pesticides. ; Trout.
Additional Subjects Insecticides ; Water analysis ; Fishes ; Gas chromatography ; Mass spectroscopy ; Residues ; Trout ; Chemical analysis ; Chlorine organic compounds ; Toxaphene ; Pesticide residues ; Biphenyl/chloro
Internet Access
Description Access URL
http://nepis.epa.gov/Exe/ZyPDF.cgi?Dockey=910170H8.PDF
Holdings
Library Call Number Additional Info Location Last
Modified
Checkout
Status
EJAD  EPA 600/3-76-076 Region 3 Library/Philadelphia, PA 06/16/2000
EJBD ARCHIVE EPA 600-3-76-076 Headquarters Library/Washington,DC 01/30/2013
EJBD  EPA 600-3-76-076 c.1 Headquarters Library/Washington,DC 03/18/2014
EKAM  EPA-600/3-76-076 Region 4 Library/Atlanta,GA 03/18/1994
ELDD  EPA-600/3-76-076 3 copies NHEERL/MED Library/Duluth,MN 08/09/2002
ESAD  EPA 600-3-76-076 Region 10 Library/Seattle,WA 03/23/2010
NTIS  PB-257 773 Most EPA libraries have a fiche copy filed under the call number shown. Check with individual libraries about paper copy. NTIS 06/23/1988
Collation ix, 43 pages : illustrations, graphs ; 28 cm.
Abstract
Sensitive methods for the detection and identification of toxaphene in water and fish are described. Polyurethane foam, gel permeation and silicic acid chromatography were used to permit accurate quantitation of multi-component toxaphene residues. A method for characterization of changes in isomer composition of toxaphene residues in fish was reported. A brief description for PCB-Toxaphene separation is given. The chemical composition of toxaphene was examined by electron impact and chemical ionization mass spectrometry. Chemical ionization gas chromatography-mass spectrometry was particularly applicable to the analysis and confirmation of toxaphene in residues in environmental samples.
Notes
Prepared by Fish-Pesticide Research Laboratory, Fish & Wildlife Service, U.S. Dept. of the Interior, Columbia, Mo., under contract no. EPA-IAG-0353 (D). Includes bibliographical references (pages 39-41). Item 431-I-11.